Glycerol 2-phosphate

Base Information

• Chemical Name: Glycerol 2-phosphate
• CAS No.: 819-83-0
• Molecular Formula: C3H9 O6 P . 2 Na
• Molecular Weight: 216.038
• Hs Code.: 2919900090
• European Community (EC) Number: 212-464-3
• Wikipedia: Glycerol_2-phosphate
• Wikidata: Q27125173
• Mol file: 819-83-0.mol

Synonyms:2-glycerophosphoric acid;beta-glycerol phosphate;beta-glycerophosphate;beta-glycerophosphoric acid;beta-glycerophosphoric acid, calcium salt;beta-glycerophosphoric acid, calcium salt (1:1);beta-glycerophosphoric acid, disodium salt;beta-glycerophosphoric acid, iron salt;beta-glycerophosphoric acid, iron(3+) salt(3:2);beta-glycerophosphoric acid, sodium salt;Glycerol 2-phosphate

Chemical Property of Glycerol 2-phosphate

Chemical Property:

• Appearance/Colour: White to cream crystalline powder
• Vapor Pressure: 1.4E-11mmHg at 25°C
• Melting Point: 102-104 °C(lit.)
• Boiling Point: 485.5 °C at 760 mmHg
• Flash Point: 247.4 °C
• PSA: 159.61000
• LogP: -0.93190
• Storage Temp.: Store at RT.
• Water Solubility.: freely soluble
• XLogP3: -3
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 3
• Exact Mass: 169.99802494
• Heavy Atom Count: 10
• Complexity: 113

Purity/Quality:

98%, ^*data from raw suppliers

beta-Glycerophosphate, 200mM soln. ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-37/39

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Chemical Classes: Metals -> Organic Acids, Metal Salts
• Canonical SMILES: C(C(CO)OP(=O)([O-])[O-])O

Technology Process of Glycerol 2-phosphate

There total 2 articles about Glycerol 2-phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

glycerol (56-81-5,25618-55-7,64333-26-2,8013-25-0) → Sodium beta-glycerophosphate (819-83-0) + disodium DL-α-glycerophosphate (1555-56-2,3325-00-6,6810-16-8,17603-42-8,35898-83-0,95648-81-0,110972-48-0,149675-96-7)

Guidance literature:

glycerol; With sodium dihydrogenphosphate; at 120 - 125 ℃; for 120h;

With sodium hydroxide; at 100 - 105 ℃; for 20h; Temperature;

Reference yield:

1,3-bis(pivaloyl)glycerol phosphate → Sodium beta-glycerophosphate (819-83-0)

Guidance literature:

With sodium hydroxide; water; at 65 ℃; pH=12 - 13;

Reference yield: 49.0%

phenyldiazomethane (908094-04-2) + triethylammonium acetate (5204-74-0) + Sodium beta-glycerophosphate (819-83-0) → C10H15O6P*0.5C6H15N

Guidance literature:

phenyldiazomethane; Sodium beta-glycerophosphate; for 0.5h; pH=6;

triethylammonium acetate; In acetonitrile; pH=7.2 - 7.3;

DOI:10.1039/c6cc03561b

upstream raw materials:

glycerol

Downstream raw materials:

4-hydroxymethyl-2-oxo-2λ⁵-[1,3,2]dioxaphospholan-2-ol

Refernces

• 1、 -. "PROCESS FOR THE SYNTHESIS OF BETA GLYCEROL PHOSPHATE". Page/Page column 23. . Retrieved 2010/08/04.