Benzoic acid, 2-[3-[2-(3-chloropropoxy)-4-(1,1-dimethylethyl)phenoxy]propoxy]-, ethyl ester

Base Information

• Chemical Name: Benzoic acid, 2-[3-[2-(3-chloropropoxy)-4-(1,1-dimethylethyl)phenoxy]propoxy]-, ethyl ester
• CAS No.: 93622-54-9
• Molecular Formula: C25H33ClO5
• Molecular Weight: 448.987
• Mol file: 93622-54-9.mol

Synonyms:

Chemical Property of Benzoic acid, 2-[3-[2-(3-chloropropoxy)-4-(1,1-dimethylethyl)phenoxy]propoxy]-, ethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzoic acid, 2-[3-[2-(3-chloropropoxy)-4-(1,1-dimethylethyl)phenoxy]propoxy]-, ethyl ester

There total 2 articles about Benzoic acid, 2-[3-[2-(3-chloropropoxy)-4-(1,1-dimethylethyl)phenoxy]propoxy]-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-tert-Butylcatechol (98-29-3) → 1-<3-(o-ethoxycarbonylphenoxy)propoxy>-2-(3-chloropropoxy)-4(5)-t-butylbenzene (93622-54-9)

Guidance literature:

Multi-step reaction with 3 steps

1: NaH

2: SOCl₂/pyridine / benzene

3: 1:1 molar ratio of educts

With pyridine; thionyl chloride; sodium hydride; In benzene;

DOI:10.1246/cl.1982.1021

Reference yield:

1,2-bis(3-hydroxypropoxy)-4-t-butylbenzene (83557-01-1) → 1-<3-(o-ethoxycarbonylphenoxy)propoxy>-2-(3-chloropropoxy)-4(5)-t-butylbenzene (93622-54-9)

Guidance literature:

Multi-step reaction with 2 steps

1: SOCl₂/pyridine / benzene

2: 1:1 molar ratio of educts

With pyridine; thionyl chloride; In benzene;

DOI:10.1246/cl.1982.1021

Reference yield: 36.0%

1-<3-(o-ethoxycarbonylphenoxy)propoxy>-2-(3-chloropropoxy)-4(5)-t-butylbenzene (93622-54-9) + 2-<3-(o-ethoxycarbonylphenoxy)propoxy>-4(5)-t-butylphenol → C47H60O10

Guidance literature:

With potassium tert-butylate; potassium iodide; In N,N-dimethyl-formamide; at 80 ℃; for 24h;

DOI:10.1246/bcsj.60.3827

upstream raw materials:

4-tert-Butylcatechol

1,2-bis(3-hydroxypropoxy)-4-t-butylbenzene

Refernces