Technology Process of Benzene,
1-chloro-5-methoxy-2-[2-(3-methoxy-2-methylphenyl)ethenyl]-4-methyl-,
(E)-
There total 5 articles about Benzene,
1-chloro-5-methoxy-2-[2-(3-methoxy-2-methylphenyl)ethenyl]-4-methyl-,
(E)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 71.1 g / HCl (gas), zinc chloride, sodium chloride / diethyl ether; H2O / 1.) 22 - 23 deg C, 2.) 12 h
2: 74.0 g / dimethylformamide / 17 h / 80 °C
3: 58.1 g / sodium hydroxide / H2O; methanol / 1.5 h / 0 °C
4: manganese dioxide / benzene / 17 h / Heating
5: methanol; dimethylformamide / 0.5 h / 90 °C
With
hydrogenchloride; manganese(IV) oxide; sodium hydroxide; sodium chloride; zinc(II) chloride;
In
methanol; diethyl ether; water; N,N-dimethyl-formamide; benzene;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: manganese dioxide / benzene / 17 h / Heating
2: methanol; dimethylformamide / 0.5 h / 90 °C
With
manganese(IV) oxide;
In
methanol; N,N-dimethyl-formamide; benzene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 74.0 g / dimethylformamide / 17 h / 80 °C
2: 58.1 g / sodium hydroxide / H2O; methanol / 1.5 h / 0 °C
3: manganese dioxide / benzene / 17 h / Heating
4: methanol; dimethylformamide / 0.5 h / 90 °C
With
manganese(IV) oxide; sodium hydroxide;
In
methanol; water; N,N-dimethyl-formamide; benzene;