Technology Process of 1,4-Benzenediol, 2-[10-(acetyloxy)decyl]-5,6-dimethoxy-3-methyl-,
1-(hydrogen sulfate), monopotassium salt
There total 4 articles about 1,4-Benzenediol, 2-[10-(acetyloxy)decyl]-5,6-dimethoxy-3-methyl-,
1-(hydrogen sulfate), monopotassium salt which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: pyridine
2: 10 percent sodium hydrosulfite / diethyl ether
3: 1.) chlorosulfonic acid, sodium hydrosulfite / pyridine / 2.) pH = 8-9
With
chlorosulfonic acid; sodium disulfite;
In
pyridine; diethyl ether;
DOI:10.1248/cpb.33.3756
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 10 percent sodium hydrosulfite / diethyl ether
2: 1.) chlorosulfonic acid, sodium hydrosulfite / pyridine / 2.) pH = 8-9
With
chlorosulfonic acid; sodium disulfite;
In
pyridine; diethyl ether;
DOI:10.1248/cpb.33.3756
- Guidance literature:
-
With
chlorosulfonic acid; sodium disulfite;
In
pyridine;
Title compound not separated from byproducts;
2.) pH = 8-9;
DOI:10.1248/cpb.33.3756
