2-Propenoic acid, 3,3'-(1,4-phenylene)bis-, didecyl ester

Base Information

• Chemical Name: 2-Propenoic acid, 3,3'-(1,4-phenylene)bis-, didecyl ester
• CAS No.: 95265-08-0
• Molecular Formula: C₃₂H₅₀O₄
• Molecular Weight: 498.747
• Mol file: 95265-08-0.mol

Synonyms:

Chemical Property of 2-Propenoic acid, 3,3'-(1,4-phenylene)bis-, didecyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-Propenoic acid, 3,3'-(1,4-phenylene)bis-, didecyl ester

There total 3 articles about 2-Propenoic acid, 3,3'-(1,4-phenylene)bis-, didecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

terephthalaldehyde, (623-27-8) → didecyl p-phenylenediacrylate (95265-08-0)

Guidance literature:

Multi-step reaction with 3 steps

1: piperidine; pyridine / 100 °C

2: thionyl chloride / Reflux

3: toluene / 80 °C

With piperidine; pyridine; thionyl chloride; In toluene;

DOI:10.1021/cg900511z

Reference yield:

1,4-phenylenediacrylic acid (16323-43-6) → didecyl p-phenylenediacrylate (95265-08-0)

Guidance literature:

Multi-step reaction with 2 steps

1: thionyl chloride / Reflux

2: toluene / 80 °C

With thionyl chloride; In toluene;

DOI:10.1021/cg900511z

Reference yield:

1-Decanol (112-30-1) + p-phenylenediacrylic diacid dichloride (35288-49-4) → didecyl p-phenylenediacrylate (95265-08-0)

Guidance literature:

In toluene; at 80 ℃;

DOI:10.1021/cg900511z

upstream raw materials:

1-Decanol

p-phenylenediacrylic diacid dichloride

1,4-phenylenediacrylic acid

terephthalaldehyde,

Refernces