Technology Process of Tetracyclo(4.2.2.26,5.01,6)dodecane
There total 5 articles about Tetracyclo(4.2.2.26,5.01,6)dodecane which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 33 percent / 50percent NaOH / hexadecyltrimethylammonium bromide / H2O; CH2Cl2; ethanol / 52 h / 5 °C
2: 86 percent / Bu3SnH / diethyl ether / 1.5 h / Heating
3: 0.61M t-BuOK / pentane; dimethylsulfoxide / 2.67 h / Ambient temperature
4: 84 percent / AgClO4 / nitromethane / 0.33 h / 0 °C
5: H2 / Pt black / ethanol
With
sodium hydroxide; potassium tert-butylate; hydrogen; tri-n-butyl-tin hydride; silver perchlorate;
cetyltrimethylammonim bromide; platinum;
In
diethyl ether; nitromethane; ethanol; dichloromethane; water; dimethyl sulfoxide; pentane;
DOI:10.1002/hlca.19860690503
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 84 percent / AgClO4 / nitromethane / 0.33 h / 0 °C
2: H2 / Pt black / ethanol
With
hydrogen; silver perchlorate;
platinum;
In
nitromethane; ethanol;
DOI:10.1002/hlca.19860690503