Technology Process of Acetic acid,
[4-chloro-2-[2-[2-(dimethoxymethyl)-5-oxocyclopentyl]ethyl]phenoxy]-,
methyl ester, trans-
There total 10 articles about Acetic acid,
[4-chloro-2-[2-[2-(dimethoxymethyl)-5-oxocyclopentyl]ethyl]phenoxy]-,
methyl ester, trans- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sulfuric acid; sodium methylate;
1) -7 to -4 deg, 30 min; 2) 30 min.;
- Guidance literature:
-
Multi-step reaction with 9 steps
1: 93 percent / 2 h / 220 - 240 °C
2: 87 percent / potassium carbonate, potassium iodide / acetone / 4 h / Heating
3: 90 percent / OsO4, potassium periodate / dioxane; H2O / 8 h
4: 2) 6 N HCl / 1) cyclohexane, reflux 4.5 h; 2) 30 deg C, 2 h.
5: 55 percent / conc. HCl / 6 h / 90 °C
6: 1.79 g / NaOH / methanol; H2O / 0.17 h / Ambient temperature
7: 88 percent / diethyl ether / 0.5 h
8: 65 percent / sodium methoxide / methanol / 40 - 50 °C
9: 86 percent / 1) sodium methoxide; 2) sulfuric acid / 1) -7 to -4 deg, 30 min; 2) 30 min.
With
hydrogenchloride; sodium hydroxide; osmium(VIII) oxide; potassium metaperiodate; sulfuric acid; sodium methylate; potassium carbonate; potassium iodide;
In
1,4-dioxane; methanol; diethyl ether; water; acetone;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 90 percent / OsO4, potassium periodate / dioxane; H2O / 8 h
2: 2) 6 N HCl / 1) cyclohexane, reflux 4.5 h; 2) 30 deg C, 2 h.
3: 55 percent / conc. HCl / 6 h / 90 °C
4: 1.79 g / NaOH / methanol; H2O / 0.17 h / Ambient temperature
5: 88 percent / diethyl ether / 0.5 h
6: 65 percent / sodium methoxide / methanol / 40 - 50 °C
7: 86 percent / 1) sodium methoxide; 2) sulfuric acid / 1) -7 to -4 deg, 30 min; 2) 30 min.
With
hydrogenchloride; sodium hydroxide; osmium(VIII) oxide; potassium metaperiodate; sulfuric acid; sodium methylate;
In
1,4-dioxane; methanol; diethyl ether; water;