Acetic acid, [[(2-hydroxyphenyl)amino]sulfinyl]-, 1,1-dimethylethyl ester

Base Information

• Chemical Name: Acetic acid, [[(2-hydroxyphenyl)amino]sulfinyl]-, 1,1-dimethylethyl ester
• CAS No.: 95778-73-7
• Molecular Formula: C12H17NO4S
• Molecular Weight: 271.337
• Mol file: 95778-73-7.mol

Synonyms:Acetic acid,[[(2-hydroxyphenyl)amino]sulfinyl]-,1,1-dimethylethyl ester;t-butyl N-(2-hydroxyphenyl)sulphinamoylacetate;tert-butyl {[(2-hydroxyphenyl)amino]sulfinyl}acetate;t-butyl N-(O-hydroxyphenyl) sulfinamoylacetate;

Chemical Property of Acetic acid, [[(2-hydroxyphenyl)amino]sulfinyl]-, 1,1-dimethylethyl ester

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Acetic acid, [[(2-hydroxyphenyl)amino]sulfinyl]-, 1,1-dimethylethyl ester

There total 1 articles about Acetic acid, [[(2-hydroxyphenyl)amino]sulfinyl]-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bromoacetic acid tert-butyl ester (5292-43-3) + N-(2-hydroxyphenyl)sulfinylamine (16932-69-7) → t-butyl N-(o-hydroxyphenyl) sulfinamoyl acetate (95778-73-7)

Guidance literature:

With zinc; In 1,2-dimethoxyethane; at 0 ℃; for 0.5h; Yield given;

DOI:10.1016/0584-8539(85)80023-4

Reference yield: 75.0%

t-butyl N-(o-hydroxyphenyl) sulfinamoyl acetate (95778-73-7) → (2-Hydroxy-phenylsulfamoyl)-acetic acid tert-butyl ester (99543-24-5)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid;

Reference yield: 25.0%

t-butyl N-(o-hydroxyphenyl) sulfinamoyl acetate (95778-73-7) → C12H15(2)H2NO4S (119421-13-5)

Guidance literature:

With sodium hydroxide; cetyltrimethylammonim bromide; In tetrahydrofuran; diethyl ether; water-d2; for 1h;

DOI:10.1039/P29880001473

upstream raw materials:

bromoacetic acid tert-butyl ester

N-(2-hydroxyphenyl)sulfinylamine

Downstream raw materials:

(2-Hydroxy-phenylsulfamoyl)-acetic acid tert-butyl ester

C₁₂H₁₅⁽²⁾H₂NO₄S

sodium t-butoxycarbonylmethanesulphinate

2-amino-phenol

Refernces