Technology Process of Aridanin
There total 9 articles about Aridanin which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside oleanolic acid;
With
sodium methylate;
In
methanol; dichloromethane;
at 20 ℃;
for 1h;
pH=10;
DOI:10.1016/j.carres.2010.01.002
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sodium hydrogencarbonate / water / 4 h / 0 - 20 °C
1.2: 0 °C
1.3: 0 °C
2.1: N-Bromosuccinimide / water; acetone / 2 h / -20 °C
2.2: 2 h / 20 °C
3.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 1 h / 0 °C / Molecular sieve
4.1: ethylenediamine / ethanol / 6 h / 80 °C
5.1: pyridine / dichloromethane / 2 h
5.2: 6 h
6.1: palladium 10% on activated carbon; hydrogen / methanol / 8 h / 20 °C
With
pyridine; N-Bromosuccinimide; trimethylsilyl trifluoromethanesulfonate; palladium 10% on activated carbon; hydrogen; sodium hydrogencarbonate; ethylenediamine;
In
methanol; ethanol; dichloromethane; water; acetone;
DOI:10.1016/j.ejmech.2017.11.004
