Technology Process of Ethanamine, 2-[4-(1,2-diphenylethenyl)phenoxy]-N,N-diethyl-, (E)-
There total 8 articles about Ethanamine, 2-[4-(1,2-diphenylethenyl)phenoxy]-N,N-diethyl-, (E)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
diphenyl acetylene;
With
diisobutylaluminium hydride;
In
hexane;
at 55 ℃;
for 18h;
4-(2-(diethylamino)ethoxy)bromobenzene;
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran;
for 24h;
Heating;
- Guidance literature:
-
4-(2-(diethylamino)ethoxy)bromobenzene;
With
magnesium; ethylene dibromide;
In
tetrahydrofuran;
With
zinc(II) chloride;
In
tetrahydrofuran;
for 0.5h;
Heating;
(E)-1-bromo-1,2-diphenylethene;
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran;
for 24h;
Heating;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) diisobutylaluminium hydride, 2.) tetrakis(triphenylphosphine) palladium / 1.) hexane, 55 deg C, 18 h, 2.) THF, reflux, 24 h
2: Ch3CH2SH, NaH / dimethylformamide / 10 h / Heating
3: sodium ethoxide / ethanol / 24 h / Heating
With
tetrakis(triphenylphosphine) palladium(0); sodium ethanolate; sodium hydride; diisobutylaluminium hydride; ethanethiol;
In
ethanol; N,N-dimethyl-formamide;