1-Propyl-2,3-diMethyliMidazoliuM broMide

Base Information

• Chemical Name: 1-Propyl-2,3-diMethyliMidazoliuM broMide
• CAS No.: 107937-17-7
• Molecular Formula: C8H15N2.Br
• Molecular Weight: 219.124
• Mol file: 107937-17-7.mol

Synonyms:1-Propyl-2,3-dimethylimidazolium bromide

Chemical Property of 1-Propyl-2,3-diMethyliMidazoliuM broMide

Chemical Property:

• PSA: 6.48000
• LogP: -1.49580

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-Propyl-2,3-diMethyliMidazoliuM broMide

There total 1 articles about 1-Propyl-2,3-diMethyliMidazoliuM broMide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,2-dimethyl-1H-imidazole (1739-84-0) + propyl bromide (106-94-5) → 1-propyl-2,3-dimethylimidazolium bromide (107937-17-7)

Guidance literature:

In cyclohexane; at 20 ℃;

DOI:10.1039/b810127b

Reference yield:

tris(bicyclo[2.2.1]heptene)platinum(0) + (1,3-dimesitylimidazol-2-ylidene)platinum(0) bis(η2-dimethylfumarate) + 1-propyl-2,3-dimethylimidazolium bromide (107937-17-7) → (platinum)(hydride)(bromide)(1,3-bis(2,4,6-trimethylphenyl)imidazolin-2-ylidene)(1,2-dimethyl-3-propylimidazole) + (platinum)(hydride)(bromide)(1,3-bis(2,4,6-trimethylphenyl)imidazolin-2-ylidene)(1,2-dimethyl-3-propylimidazole)

Guidance literature:

In acetone; 55°C;

DOI:10.1002/anie.200500884

Reference yield:

tris(bicyclo[2.2.1]heptene)platinum(0) + 1-propyl-2,3-dimethylimidazolium bromide (107937-17-7) + (platinum)(1,3-bis(2,4,6-trimethylphenyl)imidazolin-2-ylidene)(η2-styrene)2 → (platinum)(hydride)(bromide)(1,3-bis(2,4,6-trimethylphenyl)imidazolin-2-ylidene)(1,2-dimethyl-3-propylimidazole) + (platinum)(hydride)(bromide)(1,3-bis(2,4,6-trimethylphenyl)imidazolin-2-ylidene)(1,2-dimethyl-3-propylimidazole)

Guidance literature:

In acetone; 55°C;

DOI:10.1002/anie.200500884

upstream raw materials:

1,2-dimethyl-1H-imidazole

propyl bromide

Downstream raw materials:

1,2-dimethyl-3-propylimidazolium bis(trifluoromethylsulfonyl)imide

1,2-dimethyl-3-propylimidazolium tetrafluoroborate

Refernces

• 1、 Yue, Shuwen,Roveda, John D.,Mittenthal, Max S.,Shannon, Matthew S.,Bara, Jason E.. "Experimental Densities and Calculated Fractional Free Volumes of Ionic Liquids with Tri- and Tetra-substituted Imidazolium Cations". . p. 2522 - 2532. Retrieved 2018.
• 2、 Tsuda, Ryohei,Kodama, Koichi,Ueki, Takeshi,Kokubo, Hisashi,Imabayashi, Shin-Ichiro,Watanabe, Masayoshi. "LCST-type liquid-liquid phase separation behaviour of poly(ethylene oxide) derivatives in an ionic liquid". . p. 4939 - 4941. Retrieved 2008.