N-BENZOYL-DL-METHIONINE

Base Information

• Chemical Name: N-BENZOYL-DL-METHIONINE
• CAS No.: 99855-84-2
• Molecular Formula: C12H15NO3S
• Molecular Weight: 239.295
• Hs Code.: 2930909090
• Mol file: 99855-84-2.mol

Synonyms:AURORA 2284;BZ-DL-MET-OH;BZO-DL-MET-OH;BZ-DL-METHIONINE;AKOS BBS-00007545;BENZOYL-DL-METHIONINE;N-BENZOYL-DL-METHIONINE;N-ALPHA-BENZOYL-DL-METHIONINE;

Chemical Property of N-BENZOYL-DL-METHIONINE

Chemical Property:

• Melting Point: 150-154
• PSA: 91.70000
• LogP: 2.01360
• Storage Temp.: −20°C

Purity/Quality:

99%min ^*data from raw suppliers

Benzoyl-DL-methionine ^*data from reagent suppliers

Safty Information:

• Safety Statements: 24/25

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-BENZOYL-DL-METHIONINE

There total 5 articles about N-BENZOYL-DL-METHIONINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

N-Fmoc-S-methyl-L-cysteine (138021-87-1) + benzoic acid (65-85-0,8013-63-6) → N-benzoyl-S-methyl-L-cysteine (99855-84-2)

Guidance literature:

N-Fmoc-S-methyl-L-cysteine; chlorotrityl chloride (CTC) resin; With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 25 ℃;

With piperidine; In N,N-dimethyl-formamide; for 0.5h;

benzoic acid;

DOI:10.1039/c7md00409e

Reference yield:

DL-N-benzoyl-S-methylcysteine (99855-84-2) → S-methyl-L-cysteine (1187-84-4,7728-98-5) + N-benzoyl-S-methyl-L-cysteine (99855-84-2) + D-N-benzoyl-S-methylcysteine

Guidance literature:

With D-glucose; corn steep liquor; fungus Beauveria bassiana ATCC 7159; In ethanol; water; for 72h; Title compound not separated from byproducts; Enzymatic reaction;

DOI:10.1007/s007060070095

Reference yield:

S-methyl-DL-cysteine (19651-44-6,7728-98-5) + benzoyl chloride (98-88-4) → DL-N-benzoyl-S-methylcysteine (99855-84-2)

Guidance literature:

With sodium hydroxide; In water; at 20 ℃; for 2h;

DOI:10.1007/s007060070095

upstream raw materials:

S-methyl-L-cysteine

benzoyl chloride

N-Fmoc-S-methyl-L-cysteine

benzoic acid

Downstream raw materials:

S-methyl-L-cysteine

Refernces

• 1、 -. "Palatability of aquaculture feed". . . Retrieved 2008/06/13.