Technology Process of Phosphine oxide, (2,2-diethoxyethyl)bis(4-methylphenyl)-
There total 1 articles about Phosphine oxide, (2,2-diethoxyethyl)bis(4-methylphenyl)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
di(p-tolyl)phosphine oxide;
With
potassium hydride;
In
tetrahydrofuran;
for 0.5h;
Inert atmosphere;
Bromoacetaldehyde diethyl acetal;
In
tetrahydrofuran;
at 0 ℃;
for 20.0833h;
Inert atmosphere;
DOI:10.1021/om2005172
- Guidance literature:
-
With
lithium aluminium tetrahydride;
In
diethyl ether;
at 0 ℃;
for 0.75h;
Inert atmosphere;
DOI:10.1021/om2005172
- Guidance literature:
-
Multi-step reaction with 2 steps
1: lithium aluminium tetrahydride / diethyl ether / 0.75 h / 0 °C / Inert atmosphere
2: hydrogen bromide / water / Inert atmosphere
With
lithium aluminium tetrahydride; hydrogen bromide;
In
diethyl ether; water;
DOI:10.1021/om2005172
