6-NITRO-1,2-BENZISOXAZOLE

Base Information

• Chemical Name: 6-NITRO-1,2-BENZISOXAZOLE
• CAS No.: 39835-08-0
• Molecular Formula: C7H4N2O3
• Molecular Weight: 164.12
• Hs Code.: 2934999090
• Mol file: 39835-08-0.mol

Synonyms:6-NITROBENZO[D]ISOXAZOLE;6-NITRO-1,2-BENZISOXAZOLE;1,2-Benzisoxazole,6-nitro-(9CI);6-Nitroindoxazine;6-Nitro-1,2-benzisoxazol;1,2-Benzisoxazole, 6-nitro-

Chemical Property of 6-NITRO-1,2-BENZISOXAZOLE

Chemical Property:

• PSA: 71.85000
• LogP: 2.25920
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

98%,99%, ^*data from raw suppliers

6-nitrobenzo[d]isoxazole 98% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 6-NITRO-1,2-BENZISOXAZOLE

There total 2 articles about 6-NITRO-1,2-BENZISOXAZOLE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-hydroxy-4-nitrobenzaldehyde (2460-58-4) → 6-nitrobenzisoxazole (39835-08-0) + 6-nitro-1,3-benzoxazol-2-amine (6458-17-9)

Guidance literature:

With sodium azide; chloroform; sulfuric acid;

Reference yield:

→ 6-nitrobenzisoxazole (39835-08-0)

Guidance literature:

/BRN= 116616/;

Reference yield: 55.0%

6-nitrobenzisoxazole (39835-08-0) → 6-aminobenzisoxazole (828300-70-5)

Guidance literature:

With hydrogenchloride; tin(IV) chloride; tin(ll) chloride; at 20 ℃; for 5h;

DOI:10.1016/j.bmc.2006.05.071

upstream raw materials:

2-hydroxy-4-nitrobenzaldehyde

Downstream raw materials:

2-hydroxy-4-nitro-benzonitrile

6-aminobenzisoxazole