6-Bromonaphthalene-1,2-diamine

Base Information

• Chemical Name: 6-Bromonaphthalene-1,2-diamine
• CAS No.: 1241377-74-1
• Molecular Formula: C10H9BrN2
• Mol file: 1241377-74-1.mol

Synonyms:1,2-Diamino-6-bromonaphthalene;

Chemical Property of 6-Bromonaphthalene-1,2-diamine

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 6-Bromonaphthalene-1,2-diamine

There total 12 articles about 6-Bromonaphthalene-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

C10H7BrN2O2*ClH (1309945-25-2) → 6-bromo-naphthalene-1,2-diamine (1241377-74-1)

Guidance literature:

With iron; ammonium chloride; In tetrahydrofuran; water; at 60 ℃; for 3h;

Reference yield: 95.0%

6-bromo-1-nitronaphthalen-2-amine (131707-40-9) → 6-bromo-naphthalene-1,2-diamine (1241377-74-1)

Guidance literature:

With iron; ammonium chloride; In tetrahydrofuran; water; at 60 ℃; for 3h;

DOI:10.1016/j.bmcl.2016.05.042

Reference yield: 85.2%

N-acetyl-1-amino-6-bromonaphthalene → 6-bromo-naphthalene-1,2-diamine (1241377-74-1)

Guidance literature:

With hydrogenchloride; In methanol; at 55 - 65 ℃; for 5h; Industrial scale;

upstream raw materials:

N-(6-bromo-[2]naphthyl)-acetamide

6-bromo-2-naphthoic acid

6-bromo-2-aminonaphthalene hydrochloride

N-acetyl-1-nitro-6-bromonaphthalene

Downstream raw materials:

C₄₃H₅₄N₈O₆Si

C₂₉H₃₂N₆Si

C₃₉H₄₈N₆O₄Si

Refernces

• 1、 -. "Industrial preparation method of 6-bromonaphthalene-1, 2-diamine". . . Retrieved 2021/04/21.
• 2、 -. "FUSED TRICYCLIC SILYL COMPOUNDS AND METHODS OF USE THEREOF FOR THE TREATMENT OF VIRAL DISEASES". . . Retrieved 2015/12/08.