2-Methyladamantan-2-yl acrylate

Base Information

• Chemical Name: 2-Methyladamantan-2-yl acrylate
• CAS No.: 249562-06-9
• Molecular Formula: C14H20O2
• Molecular Weight: 220.312
• Hs Code.: 2916129000
• European Community (EC) Number: 835-735-3
• DSSTox Substance ID: DTXSID10947831
• Nikkaji Number: J2.018.499J
• Wikidata: Q72486552
• Mol file: 249562-06-9.mol

Synonyms:249562-06-9;2-Methyladamantan-2-yl acrylate;2-methyl-2-adamantyl acrylate;(2-methyl-2-adamantyl) Prop-2-enoate;2-METHYLADAMANTAN-2-YL PROP-2-ENOATE;2-Propenoic acid, 2-methyltricyclo[3.3.1.13,7]dec-2-yl ester;2-Methyladamantan-2-yl Acrylate (stabilized with MEHQ);2-Propenoic acid, 2-methyltricyclo(3.3.1.13,7)dec-2-yl ester;SCHEMBL39900;2-Methyladamantan-2-ylacrylate;SCHEMBL13359045;SCHEMBL14445497;DTXSID10947831;YRPLSAWATHBYFB-UHFFFAOYSA-N;AMY11180;MFCD08704223;AKOS015900782;Acrylic acid 2-methyl-2-adamantyl ester;AC-32092;AS-70994;FT-0646061;M3223;D91626;A817571;2-Methyladamantan-2-yl Acrylate, >/=98%,stabilized with MEHQ

Chemical Property of 2-Methyladamantan-2-yl acrylate

Chemical Property:

• Vapor Pressure: 0.00298mmHg at 25°C
• Refractive Index: 1.52
• Boiling Point: 284.426 °C at 760 mmHg
• Flash Point: 114.556 °C
• PSA: 26.30000
• Density: 1.076 g/cm³
• LogP: 2.93040
• Storage Temp.: 2-8°C
• XLogP3: 3.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 3
• Exact Mass: 220.146329876
• Heavy Atom Count: 16
• Complexity: 304

Purity/Quality:

99%min ^*data from raw suppliers

2-Methyladamantan-2-yl Acrylate (stabilized with MEHQ) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CC1(C2CC3CC(C2)CC1C3)OC(=O)C=C

Technology Process of 2-Methyladamantan-2-yl acrylate

There total 3 articles about 2-Methyladamantan-2-yl acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

2-methyladamantan-2-ol (702-98-7) + acryloyl chloride (814-68-6,25189-84-8) → acrylic acid-2-methyl-2-adamantyl (249562-06-9)

Guidance literature:

With triethylamine; In butanone; at 60 - 77 ℃; for 3h;

Reference yield: 91.5%

2-methylideneadamantane (875-72-9) + acrylic acid (79-10-7) → acrylic acid-2-methyl-2-adamantyl (249562-06-9)

Guidance literature:

With sodium hydroxide; sulfuric acid; In toluene;

Reference yield:

→ acrylic acid-2-methyl-2-adamantyl (249562-06-9)

Guidance literature:

upstream raw materials:

2-methyladamantan-2-ol

acryloyl chloride

2-methylideneadamantane

acrylic acid

Downstream raw materials:

5-norbornene-2-(2-methyl-2-adamantyl)carboxylate

Refernces

• 1、 -. "Processes for preparation of 2-alkyl-2adamantyl esters". . . Retrieved 2008/06/13.
• 2、 -. "Process for producing a 2-adamantyl (meth>acrylate". Example 2. . Retrieved 2008/06/13.