Potassium 6-chloropyridine-3-trifluoroborate

Base Information

• Chemical Name: Potassium 6-chloropyridine-3-trifluoroborate
• CAS No.: 1235099-38-3
• Molecular Formula: C5H3BClF3KN
• Molecular Weight: 219.443
• Hs Code.: 2933399990
• Mol file: 1235099-38-3.mol

Synonyms:potassium,(6-chloropyridin-3-yl)-trifluoroboranuide;

Chemical Property of Potassium 6-chloropyridine-3-trifluoroborate

Chemical Property:

• Melting Point: 298-303 °C
• PSA: 12.89000
• LogP: 1.78940
• Storage Temp.: Inert atmosphere,Room Temperature

Purity/Quality:

98.5% ^*data from raw suppliers

Potassium 6-chloropyridine-3-trifluoroborate ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xn
• Hazard Codes: Xn
• Statements: 22-36/37/38
• Safety Statements: 26

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Potassium 6-chloropyridine-3-trifluoroborate

There total 1 articles about Potassium 6-chloropyridine-3-trifluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

6-chloropyridin-3-ylboronic acid (444120-91-6) → potassium (6-chloropyridin-3-yl)trifluoroborate (1235099-38-3)

Guidance literature:

With potassium hydrogen difluoride; In methanol; water; Cooling with ice; Inert atmosphere;

DOI:10.1021/ol101067d

Reference yield: 91.0%

potassium (6-chloropyridin-3-yl)trifluoroborate (1235099-38-3) → 6-chloropyridine-3-ol (41288-96-4)

Guidance literature:

With Oxone; water; In acetone; at 20 ℃; for 0.0833333h;

DOI:10.1021/jo102208d

upstream raw materials:

6-chloropyridin-3-ylboronic acid

Downstream raw materials:

6-chloropyridine-3-ol

Refernces