Technology Process of 1-Bromotetracosane
There total 8 articles about 1-Bromotetracosane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N-Bromosuccinimide; triphenylphosphine;
In
dichloromethane;
at 20 ℃;
for 5h;
DOI:10.1016/j.tet.2005.09.056
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 78 percent / n-BuLi / hexamethylphosphoric acid triamide
2: ethylenediamine, NaH / 45 - 55 °C
3: 1.) n-BuLi / 1.) HMPA. 2.) HMPA
4: H2 / Pd/C / ethanol
5: 48percent aq. HBr, conc. H2SO4 / 90 - 110 °C
With
n-butyllithium; sulfuric acid; hydrogen bromide; hydrogen; sodium hydride; ethylenediamine;
palladium on activated charcoal;
In
N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol;
DOI:10.1021/ja00062a086
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) n-BuLi / 1.) HMPA. 2.) HMPA
2: H2 / Pd/C / ethanol
3: 48percent aq. HBr, conc. H2SO4 / 90 - 110 °C
With
n-butyllithium; sulfuric acid; hydrogen bromide; hydrogen;
palladium on activated charcoal;
In
ethanol;
DOI:10.1021/ja00062a086
