(E)-10-Hexadecenal

Base Information

• Chemical Name: (E)-10-Hexadecenal
• CAS No.: 72698-30-7
• Molecular Formula: C₁₆H₃₀O
• Molecular Weight: 238.414
• Mol file: 72698-30-7.mol

Synonyms:(E)-10-Hexadecenal;(10E)-10-Hexadecenal;E10-16CHO

Chemical Property of (E)-10-Hexadecenal

Chemical Property:

• PSA: 17.07000
• LogP: 5.44260

Purity/Quality:

98%,99%, ^*data from raw suppliers

(E)-10-Hexadecenal ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: (E)-10-Hexadecenal is an aliphatic aldehyde that has been identified as a sex pheromone component of the yellow peach moth, Dichocrocis punctiferalis Guenee.

Technology Process of (E)-10-Hexadecenal

There total 6 articles about (E)-10-Hexadecenal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

10-hexadecenol → (E)-10-hexadecenal (72698-30-7)

Guidance literature:

With pyridinium chlorochromate; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;

Reference yield: 61.0%

(E/Z)-10-hexadecen-1-ol (86416-30-0) → (E/Z)-10-hexadecenal (72698-30-7)

Guidance literature:

With pyridinium chlorochromate; In dichloromethane; for 1h;

Reference yield:

10-oxo-decanoic acid methyl ester (14811-73-5) → (E/Z)-10-hexadecenal (72698-30-7)

Guidance literature:

Multi-step reaction with 3 steps

1: 1.) n-BuLi / 1.) ether, hexane, 1 h, 2.) ether, hexane, a.) -40 deg C, 1 h, b.) RT, 6 h

2: 71 percent / LAH / diethyl ether / 1 h / Heating

3: 61 percent / PCC / CH₂Cl₂ / 1 h

With lithium aluminium tetrahydride; n-butyllithium; pyridinium chlorochromate; In diethyl ether; dichloromethane;

upstream raw materials:

(E/Z)-10-hexadecen-1-ol

10-oxo-decanoic acid methyl ester

10,11-dihydroxyundecanoic acid

methyl 10,11-dihydroxyundecanoate

Refernces

• 1、 Hassarajani, S. A.,Subaraman, A. S.,Mamdapur, V. R.. "FACILE SYNTHESIS OF PHEROMONE OF Dichocrocis Punctiferalis, A SERIOUS PEST OF SPICES". . p. 571 - 573. Retrieved 2007/10/02.