3-Hydroxyphenylglyoxal

Base Information Edit

Chemical Name:3-Hydroxyphenylglyoxal
CAS No.:70935-14-7
Molecular Formula:C8H6O3
Molecular Weight:150.134
Hs Code.:
Mol file:70935-14-7.mol

Synonyms:2-(3-hydroxyphenyl)-2-oxoacetaldehyde;3-hydroxyphenylglyoxal;70935-14-7;(3-Hydroxyphenyl)glyoxal;SCHEMBL3539849;BFHONQWJUMCAKI-UHFFFAOYSA-N;EN300-190266;Z1255357387

Suppliers and Price of 3-Hydroxyphenylglyoxal

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 3-Hydroxyphenylglyoxal Edit

Chemical Property:

PSA：54.37000
LogP:0.77380
XLogP3:1.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:150.031694049
Heavy Atom Count:11
Complexity:165

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC(=C1)O)C(=O)C=O

Technology Process of 3-Hydroxyphenylglyoxal

There total 3 articles about 3-Hydroxyphenylglyoxal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 121-71-1
3-Hydroxyacetophenone

: 70935-14-7
3-hydroxyphenylglyoxal

Guidance literature:: With sodium hydroxide; potassium hexacyanoferrate(III); In water; at 30 ℃; Kinetics; Mechanism; Thermodynamic data; E_a, ΔS(excit.), ΔG(excit.);

Reference yield:

: 7446-08-4
selenium(IV) oxide

: 121-71-1
3-Hydroxyacetophenone

: 70935-14-7
3-hydroxyphenylglyoxal

Guidance literature:

Reference yield:

: 100-83-4
meta-hydroxybenzaldehyde

: 70935-14-7
3-hydroxyphenylglyoxal

Guidance literature:: Multi-step reaction with 2 steps

1.1: 3-ethylbenzothiazolium bromide; triethylamine / ethanol / 24 h / 60 °C

2.1: copper(I) tetrakis(acetonitrile) hexafluorophosphate / 0.5 h / Molecular sieve; Schlenk technique

2.2: 0.5 h / 20 °C / 760.05 Torr / Schlenk technique; Molecular sieve

With copper(I) tetrakis(acetonitrile) hexafluorophosphate; triethylamine; 3-ethylbenzothiazolium bromide; In ethanol;
DOI:10.1039/d2cc00773h