p-Toluidine, nitrate

Base Information

• Chemical Name: p-Toluidine, nitrate
• CAS No.: 32954-54-4
• Molecular Formula: C7H10N2O3
• Molecular Weight: 170.168
• Hs Code.: 2921430090
• Mol file: 32954-54-4.mol

Synonyms:

Chemical Property of p-Toluidine, nitrate

Chemical Property:

• Boiling Point: 197.4°Cat760mmHg
• Flash Point: 84.5°C
• PSA: 92.07000
• Density: g/cm³
• LogP: 2.33390

Purity/Quality:

P-TOLUIDINE, NITRATE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of p-Toluidine, nitrate

There total 2 articles about p-Toluidine, nitrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl nitrate (625-58-1) + p-toluidine (106-49-0,12221-03-3) → para-methyl anilinium nitrate (32954-54-4) + N-ethyl-p-tolylamine (622-57-1)

Guidance literature:

at 100 ℃;

Reference yield:

butyl nitrate (928-45-0) + p-toluidine (106-49-0,12221-03-3) → N-butyl-4-methylaniline (10387-24-3) + para-methyl anilinium nitrate (32954-54-4)

Guidance literature:

at 100 ℃;

Reference yield:

para-methyl anilinium nitrate (32954-54-4) → 4-methyl-2-nitroaniline (89-62-3)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic acid anhydride

2: HCl; diethyl ether

With hydrogenchloride; diethyl ether; acetic anhydride;

upstream raw materials:

ethyl nitrate

p-toluidine

butyl nitrate

Downstream raw materials:

1-(4-tolyl)guanidine

4-Methylacetanilide

4-methyl-2-nitroaniline

N-nitro-p-toluidine