Technology Process of (9Z)-3-Oxo-9-hexadecenal
There total 5 articles about (9Z)-3-Oxo-9-hexadecenal which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium;
In
benzene;
1.) room temp., 1 h, 2.) reflux, 1 h;
DOI:10.1021/jo00324a035
- Guidance literature:
-
Multi-step reaction with 4 steps
1: pyridium chlorochromate / CH2Cl2 / 3 h / 20 °C
2: tetrahydrofuran; diethyl ether / 2 h / 0 - 20 °C
3: Jones reagent, 2-propanol / acetone
4: 44 percent / Na / benzene / 1.) room temp., 1 h, 2.) reflux, 1 h
With
jones reagent; sodium; isopropyl alcohol;
In
tetrahydrofuran; diethyl ether; dichloromethane; acetone; benzene;
DOI:10.1021/jo00324a035
- Guidance literature:
-
Multi-step reaction with 5 steps
1: aq. K2CO3 / ethanol / 16 h
2: pyridium chlorochromate / CH2Cl2 / 3 h / 20 °C
3: tetrahydrofuran; diethyl ether / 2 h / 0 - 20 °C
4: Jones reagent, 2-propanol / acetone
5: 44 percent / Na / benzene / 1.) room temp., 1 h, 2.) reflux, 1 h
With
jones reagent; sodium; potassium carbonate; isopropyl alcohol;
In
tetrahydrofuran; diethyl ether; ethanol; dichloromethane; acetone; benzene;
DOI:10.1021/jo00324a035
