Perovskite CH3NH3PbBr3 Powder

Base Information

• Chemical Name: Perovskite CH3NH3PbBr3 Powder
• CAS No.: 69276-13-7
• Molecular Formula: CH5N.PbBr3.H
• Molecular Weight: 482
• Mol file: 69276-13-7.mol

Synonyms:CH3NH3PbBr3;Perovskite CH3NH3PbBr3 Powder;Methylammonium tribromoplumbate

Chemical Property of Perovskite CH3NH3PbBr3 Powder

Chemical Property:

• PSA: 26.02000
• LogP: 2.43120

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Perovskite CH3NH3PbBr3 Powder

There total 6 articles about Perovskite CH3NH3PbBr3 Powder which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

lead(II) bromide + methylammonium bromide (6876-37-5) → methylammonium lead bromide (69276-13-7)

Guidance literature:

In N,N-dimethyl-formamide; under N2; stoich. amts.; soln. of alkylammonium salt and Pb salt in DMF at room temp.; soln. poured into acetone; elem. anal.;

DOI:10.1246/bcsj.79.1607

Reference yield:

PbBr3 + methylamine (74-89-5) → methylammonium lead bromide (69276-13-7)

Guidance literature:

PbBr₃; methylamine; In ethanol; at 20 ℃; for 0.000833333h;

at 80 ℃; for 0.0166667h;

DOI:10.1039/c6cc05794b

Reference yield:

lead acetate (301-04-2) + methylammonium bromide (6876-37-5) → methylammonium lead bromide (69276-13-7)

Guidance literature:

In water; Drop-by-drop addn. of aq. soln. of Pb-compd. to excess of hot aq. soln. of org. compd. and slow cooling to about 5°C.; Elem. anal. of obtained crystals.;

DOI:10.1016/0022-3697(90)90021-7

upstream raw materials:

hydrogen bromide

lead acetate

methylamine

methylammonium bromide

Refernces

• 1、 Takeoka, Yuko,Asai, Keisuke,Rikukawa, Masahiro,Sanui, Kohei. "Systematic studies on chain lengths, halide species, and well thicknesses for lead halide layered perovskite thin films". . p. 1607 - 1613. Retrieved 2006.
• 2、 Nayak, Pabitra K.,Sendner, Michael,Wenger, Bernard,Wang, Zhiping,Sharma, Kshama,Ramadan, Alexandra J.,Lovrin?i?, Robert,Pucci, Annemarie,Madhu,Snaith, Henry J.. "Impact of Bi3+ Heterovalent Doping in Organic-Inorganic Metal Halide Perovskite Crystals". . p. 574 - 577. Retrieved 2018.
• 3、 Onoda-Yamamuro, Noriko,Matsuo, Takasuke,Suga, Hiroshi. "Calorimetric and IR spectroscopic studies of phase transitions in methylammonium trihalogenoplumbates (II)". . p. 1383 - 1396. Retrieved 1990.
• 4、 Sardar, Soumen,Jana, Atanu,Mukherjee, Avik,Dhara, Anamika,Bandyopadhyay, Abhijit. "Bottom-up synthesis of bright fluorescent, moisture-resistant methylammonium lead bromide@poly(3-bromothiophene)". . p. 2053 - 2058. Retrieved 2020/02/13.