Technology Process of CID 53425746
There total 5 articles about CID 53425746 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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In
neat (no solvent);
React. (vac. line, no solvent) at room temp. for 10 min.; Removal of Me3SnCl by passing the mixt. through a trap cooled to -95°C (toluene). IR and NMR spectra indicate presence of resulting compounds in approximately equimolar amt.;
- Guidance literature:
-
In
neat (no solvent);
React. of equimolar amt. of starting materials (vac. line, room temp., 10 min).; Removal of Me3SnCl by passing the mixt. through a trap cooled to -95°C (toluene). IR identificatio of resulting compounds.;
- Guidance literature:
-
In
neat (no solvent);
Warming mixt. of equimolar amt. of starting materials (condensed at -196°C) to -80°C (30 min) and then gradually to 10°C.; Removal of Me3SnCl by passing the mixt. through a trap cooled to -95°C (toluene). NMR spectrum indicate presence of major resulting compounds, with small amt. of SiF3SiHBr2 and unreacted SiF3SiFHBr.;
