6α-Acetoxy-5α-androstane

Base Information

• Chemical Name: 6α-Acetoxy-5α-androstane
• CAS No.: 35487-67-3
• Molecular Formula: C21H34O2
• Molecular Weight: 318.49346
• Mol file: 35487-67-3.mol

Synonyms:6α-Acetoxy-5α-androstane

Chemical Property of 6α-Acetoxy-5α-androstane

Chemical Property:

• PSA: 26.30000
• LogP: 5.35090

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 6α-Acetoxy-5α-androstane

There total 3 articles about 6α-Acetoxy-5α-androstane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 6β-Acetoxy-androstan (35487-67-3,35487-68-4,35494-33-8)

Guidance literature:

Aus 6β-Androstanol mit Essigsaeureanhydrid;

DOI:10.1021/jo00863a016

Reference yield:

(5α)-androstane (438-22-2,28805-72-3) + acetic acid (64-19-7,77671-22-8) → 12α-Acetoxy-5α-androstan (35487-69-5) + 6α-Acetoxy-5α-androstan (35487-67-3) + 7α-Acetoxy-5α-androstan (22033-64-3)

Guidance literature:

In dichloromethane; at 20 ℃; Yield given. Yields of byproduct given;

Reference yield:

→ 6α-Acetoxy-5α-androstan (35487-67-3)

Guidance literature:

aus entspr.Alkohol (XXI),Ac2O/Py.;

upstream raw materials:

(5α)-androstane

acetic acid

Refernces

• 1、 Eggert,VanAntwerp,Bhacca,Djerassi. "Carbon-13 nuclear magnetic resonance spectra of hydroxy steroids.". . p. 71 - 78. Retrieved 2007/10/12.