1,9-Dinitrophenazine

Base Information

• Chemical Name: 1,9-Dinitrophenazine
• CAS No.: 58718-48-2
• Molecular Formula: C12H6N4O4
• Molecular Weight: 270.2
• Mol file: 58718-48-2.mol

Synonyms:1,9-Dinitro-phenazin;1,9-dinitro-phenazine;UBAQDYYJIKENDK-UHFFFAOYSA;

Chemical Property of 1,9-Dinitrophenazine

Chemical Property:

• Vapor Pressure: 4.88E-10mmHg at 25°C
• Boiling Point: 510.6°C at 760 mmHg
• Flash Point: 262.6°C
• PSA: 117.42000
• Density: 1.61g/cm³
• LogP: 3.64580

Purity/Quality:

99%min ^*data from raw suppliers

1,9-DINITROPHENAZINE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,9-Dinitrophenazine

There total 4 articles about 1,9-Dinitrophenazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

Phenazin (92-82-0) → 1,9-dinitrophenazine (58718-48-2) + 1,6-dinitrophenazine (36848-41-6)

Guidance literature:

With XNO₂;

DOI:10.1016/S0040-4020(98)01128-4

Reference yield:

Phenazin (92-82-0) → 1,9-dinitrophenazine (58718-48-2)

Guidance literature:

With sulfuric acid; nitric acid; for 0.5h; Heating;

DOI:10.1021/ja035212l

Reference yield:

Phenazin (92-82-0) → 2-nitrophenazine (3442-62-4) + 1,3-dinitro-phenazine (13860-47-4) + 1,9-dinitrophenazine (58718-48-2) + 2,9-dinitrophenazine

Guidance literature:

With sulfuric acid; nitric acid; at 50 ℃; for 96h;

DOI:10.3390/biom11111728

upstream raw materials:

Phenazin

Downstream raw materials:

1,9-diaminophenazine

Refernces

• 1、 Mateo Alonso,Horcajada, Roberto,Groombridge, Helen J.,Chudasama, Reshma,Motevalli, Majid,Utley, James H. P.,Wyatt, Peter B.. "Synthesis of phenazine derivatives for use as precursors to electrochemically generated bases". . p. 2832 - 2841. Retrieved 2007/10/03.
• 2、 Huszthy, Peter,Samu, Erika,Vermes, Borbala,Mezey-Vandor, Gabriella,Nogradi, Mihaly,Bradshaw, Jerald S.,Izatt, Reed M.. "Synthesis of novel acridino- and phenazino-18-crown-6 ligands and their optically pure dimethyl-substituted analogues for molecular recognition studies". . p. 1491 - 1504. Retrieved 2007/10/03.