4-Hydroxybenzoic-1,2,3,4,5,6-13C6 Acid

Base Information

• Chemical Name: 4-Hydroxybenzoic-1,2,3,4,5,6-13C6 Acid
• CAS No.: 287399-29-5
• Molecular Formula: C7H6O3
• Molecular Weight: 144.17474
• Mol file: 287399-29-5.mol

Synonyms:4-Hydroxybenzoic-1,2,3,4,5,6-13C6 Acid;4-Hydroxybenzoic acid-(phenyl-13C6)

Chemical Property of 4-Hydroxybenzoic-1,2,3,4,5,6-13C6 Acid

Chemical Property:

• PSA: 57.53000
• LogP: 1.09040
• Storage Temp.: Refrigerator, under inert atmosphere
• Solubility.: DMSO (Slightly), Methanol (Slightly)

Purity/Quality:

NLT 98% ^*data from raw suppliers

4-Hydroxybenzoic-1,2,3,4,5,6-13C6 Acid ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 4-Hydroxybenzoic-1,2,3,4,5,6-13C6 Acid is the isotope labelled analog of 4-Hydroxybenzoic Acid (S088120); the Impurity A of Acetylsalicylic Acid.

Technology Process of 4-Hydroxybenzoic-1,2,3,4,5,6-13C6 Acid

There total 1 articles about 4-Hydroxybenzoic-1,2,3,4,5,6-13C6 Acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.65%

tetrachloromethane (56-23-5) + [13C6]phenol (89059-34-7) → p-hydroxybenzoic acid-13C6 (287399-29-5)

Guidance literature:

[¹³C₆]phenol; With water; β‐cyclodextrin; sodium hydroxide; copper dichloride; for 0.5h;

tetrachloromethane; at 110 ℃; for 13h; Temperature; Reagent/catalyst;

upstream raw materials:

tetrachloromethane

[¹³C₆]phenol

Refernces