Fmoc-DL-Asu-OH

Base Information

• Chemical Name: Fmoc-DL-Asu-OH
• CAS No.: 1208999-99-8
• Molecular Formula: C₂₃H₂₅NO₆
• Molecular Weight: 411.455
• Mol file: 1208999-99-8.mol

Synonyms:Fmoc-DL-Asu-OH

Chemical Property of Fmoc-DL-Asu-OH

Chemical Property:

• Boiling Point: 670.9±55.0 °C(Predicted)
• PKA: 3.89±0.21(Predicted)
• PSA: 112.93000
• Density: 1.286±0.06 g/cm3(Predicted)
• LogP: 4.40430

Purity/Quality:

99.3% ^*data from raw suppliers

Fmoc-DL-Asu-OH ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Fmoc-DL-Asu-OH

There total 1 articles about Fmoc-DL-Asu-OH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-amino-octanedioic acid (3054-07-7,19641-59-9) + (fluorenylmethoxy)carbonyl chloride (28920-43-6) → 2-(((9H-fluoren-9-yl)methoxy)carbonylamino)octanedioic acid (1208999-99-8,218457-78-4)

Guidance literature:

2-amino-octanedioic acid; With potassium carbonate; In water;

(fluorenylmethoxy)carbonyl chloride; In 1,4-dioxane; water;

Reference yield:

2-(((9H-fluoren-9-yl)methoxy)carbonylamino)octanedioic acid (1208999-99-8,218457-78-4) → C44H67N13O14S2 (1208999-98-7)

Guidance literature:

Multi-step reaction with 2 steps

1: ethyl acetate; dicyclohexyl-carbodiimide / 8 h / 0 °C

2: N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide / 24 h / 20 °C

With ethyl acetate; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; In dimethyl sulfoxide;

upstream raw materials:

2-amino-octanedioic acid

(fluorenylmethoxy)carbonyl chloride

Downstream raw materials:

C₄₄H₆₇N₁₃O₁₄S₂

Refernces