8-epideoxyloganic acid

Base Information

• Chemical Name: 8-epideoxyloganic acid
• CAS No.: 88668-99-9
• Molecular Formula: C16H24O9
• Molecular Weight: 360.36
• Mol file: 88668-99-9.mol

Synonyms:8-epideoxyloganic acid

Chemical Property of 8-epideoxyloganic acid

Chemical Property:

• Boiling Point: 597.2±50.0 °C(Predicted)
• PKA: 4.65±0.60(Predicted)
• PSA: 145.91000
• Density: 1.52±0.1 g/cm3(Predicted)
• LogP: -1.21000

Purity/Quality:

98%Min ^*data from raw suppliers

8-EpideoxyloganicAcid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 8-epideoxyloganic acid

There total 1 articles about 8-epideoxyloganic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 7-desoxyloganic Saeure (22487-36-1,86363-69-1,88668-99-9)

Guidance literature:

aus XII;

Reference yield:

1,5,9-epideoxyloganic acid (22487-36-1,86363-69-1,88668-99-9) → (-)-boschnialactone (17957-87-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 416 mg / β-glucosidase, H2O / 24 h / 37 °C

2: 2 N KOH / ethanol / 3 h / Heating

3: 10 percent H₂SO₄ / ethanol / 0.5 h / Heating

With potassium hydroxide; sulfuric acid; water; β-glucosidase; In ethanol;

DOI:10.1248/cpb.32.2809

Reference yield:

diazomethane (186581-53-3,908094-01-9,334-88-3) + 1,5,9-epideoxyloganic acid (22487-36-1,86363-69-1,88668-99-9) → 1,5,9-epideoxyloganic acid methyl ester (26660-57-1,78216-56-5,86363-70-4,92842-57-4)

Guidance literature:

In diethyl ether;

DOI:10.1248/cpb.32.2809

Downstream raw materials:

1,5,9-epideoxyloganic acid methyl ester

(1S,4aS,7R,7aR)-7-Methyl-1-((2R,3S,4R,5R,6S)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-1,4a,5,6,7,7a-hexahydro-cyclopenta[c]pyran-4-carboxylic acid methyl ester

ipolamiide

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