Technology Process of 5-Phenoxypentanoic acid ethyl ester
There total 4 articles about 5-Phenoxypentanoic acid ethyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tris-(dibenzylideneacetone)dipalladium(0); 2-methyl-but-2-ene; hydrogen; 1,4-di(diphenylphosphino)-butane;
In
chloroform;
at 120 ℃;
for 36h;
under 31029.7 Torr;
regioselective reaction;
Schlenk technique;
Inert atmosphere;
Autoclave;
DOI:10.1021/acs.joc.6b00522
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate / acetone / 12 h / 66 °C
2: tris-(dibenzylideneacetone)dipalladium(0); 1,4-di(diphenylphosphino)-butane; 2-methyl-but-2-ene; hydrogen / chloroform / 36 h / 120 °C / 31029.7 Torr / Schlenk technique; Inert atmosphere; Autoclave
With
tris-(dibenzylideneacetone)dipalladium(0); 2-methyl-but-2-ene; hydrogen; potassium carbonate; 1,4-di(diphenylphosphino)-butane;
In
chloroform; acetone;
DOI:10.1021/acs.joc.6b00522
