2-Carene epoxide

Base Information

• Chemical Name: 2-Carene epoxide
• CAS No.: 20053-58-1
• Molecular Formula: C10H16O
• Molecular Weight: 152.236
• Hs Code.: 2932999099
• Mol file: 20053-58-1.mol

Synonyms:2-Carene epoxide

Chemical Property of 2-Carene epoxide

Chemical Property:

• Boiling Point: 63 °C(Press: 7 Torr)
• PSA: 12.53000
• Density: 1.027±0.06 g/cm3(Predicted)
• LogP: 2.20990

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Carene epoxide

There total 5 articles about 2-Carene epoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

2-carene (4497-92-1) → (1S,2S,3R,6R)-(+)-trans-car-2-ene epoxide (20053-58-1)

Guidance literature:

With 3,3-dimethyldioxirane; In dichloromethane; acetone; at -5 ℃; for 1h;

DOI:10.1055/s-2001-18751

Reference yield:

(+)-Δ3-carene (498-15-7,19079-29-9) + 2-carene (4497-92-1) → (1S,2S,3R,6R)-(+)-trans-car-2-ene epoxide (20053-58-1) + 3-carene epoxide (936-91-4)

Guidance literature:

With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; water; at 23 - 32 ℃; for 2.08333h; Product distribution / selectivity;

Reference yield:

(+)-Δ3-carene (498-15-7,19079-29-9) → (1S,2S,3R,6R)-(+)-trans-car-2-ene epoxide (20053-58-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 15 percent / potassium t-butoxide / dimethylsulfoxide / 4 h / 100 °C

2: 80percent m-chloroperoxybenzoic acid / diethyl ether / 24 h / 0 °C

With potassium tert-butylate; 3-chloro-benzenecarboperoxoic acid; In diethyl ether; dimethyl sulfoxide;

DOI:10.1039/P19880001243

upstream raw materials:

2-carene

(+)-Δ³-carene

Downstream raw materials:

cis-Δ²-p-menthene-1,8-diol

(1R,4R)-p-mentha-2,8-dien-1-ol

delta-8-tetrahydrocannabinol

dronabinol

Refernces

• 1、 Scianowski, Jacek,Rafinski, Zbigniew,Wojtczak, Andrzej,Burczynski, Krzysztof. "Syntheses and reactions of terpene β-hydroxyselenides and β-hydroxydiselenides". body text. p. 2871 - 2879. Retrieved 2010/03/30.
• 2、 -. "METHODS AND INTERMEDIATES FOR THE SYNTHESIS OF DELTA-9 TETRAHYDROCANNABINOL". Page/Page column title page; 3/7. . Retrieved 2008/06/13.