2-cycloheptylideneethanol

Base Information Edit

Chemical Name:2-cycloheptylideneethanol
CAS No.:4448-83-3
Molecular Formula:C₉H₁₆O
Molecular Weight:140.225
Hs Code.:
Mol file:4448-83-3.mol

Synonyms:

Suppliers and Price of 2-cycloheptylideneethanol

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 2-cycloheptylideneethanol Edit

Chemical Property:

Vapor Pressure:0.0299mmHg at 25°C
Boiling Point:216.6°Cat760mmHg
Flash Point:94.4°C
Density:1.009g/cm³

Purity/Quality:: 99%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-cycloheptylideneethanol

There total 8 articles about 2-cycloheptylideneethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1903-23-7
ethyl cycloheptylideneacetate

: 4448-83-3
α-(hydroxymethyl)methylenecycloheptane

Guidance literature:: ethyl cycloheptylideneacetate; With diisobutylaluminium hydride; In dichloromethane; at -78 - 20 ℃; for 3h;

With water; sodium hydroxide;
DOI:10.1021/ja4047312

Reference yield: 83.0%

: 1903-29-3
cycloheptylideneacetic acid

: 4448-83-3
α-(hydroxymethyl)methylenecycloheptane

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; for 0.333333h;

Reference yield: 58.0%

: C₁₆H₃₃IOSi

: 21336-32-3
1-(2-hydroxyethyl)cyclohept-1-ene

: 4448-83-3
α-(hydroxymethyl)methylenecycloheptane

: 172606-13-2
2-(cyclohept-2-en-1-yl)ethanol

Guidance literature:: C₁₆H₃₃IOSi; With 1-(diphenylphosphino)ferrocene-1-(di-tert-butylphosphino)ferrocene; palladium diacetate; caesium carbonate; In benzene; at 20 ℃; Inert atmosphere; Glovebox; Irradiation;

With tetrabutyl ammonium fluoride; In tetrahydrofuran; benzene; at 20 ℃; Overall yield = 71 %; regioselective reaction; Inert atmosphere; Glovebox;
DOI:10.1021/jacs.7b08459