Methyl 3-broMo-4-cyanobenzoate

Base Information Edit

Chemical Name:Methyl 3-broMo-4-cyanobenzoate
CAS No.:942598-44-9
Molecular Formula:C9H6BrNO2
Molecular Weight:240.056
Hs Code.:2926909090
Mol file:942598-44-9.mol

Synonyms:Methyl 3-broMo-4-cyanobenzoate

Suppliers and Price of Methyl 3-broMo-4-cyanobenzoate

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

AHH
methyl3-bromo-4-cyanobenzoate 97%
1g
$ 950.00

AK Scientific
Methyl3-bromo-4-cyanobenzoate
10g
$ 1651.00

Alichem
Methyl3-bromo-4-cyanobenzoate
1g
$ 1534.70

Alichem
Methyl3-bromo-4-cyanobenzoate
250mg
$ 499.20

American Custom Chemicals Corporation
METHYL-3-BROMO-4-CYANOBENZOATE 95.00%
5MG
$ 504.52

Total 8 raw suppliers

Chemical Property of Methyl 3-broMo-4-cyanobenzoate Edit

Chemical Property:

PSA：50.09000
LogP:2.10738
Storage Temp.:2-8°C

Purity/Quality:

98%Min ^*data from raw suppliers

methyl3-bromo-4-cyanobenzoate 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses Methyl 3-bromo-4-cyanobenzoate is used as a reactant in the palladium-?catalyzed highly selective ortho-?halogenation of arylnitriles.

Technology Process of Methyl 3-broMo-4-cyanobenzoate

There total 4 articles about Methyl 3-broMo-4-cyanobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1129-35-7
4-cyanobenzoic acid methyl ester

: 942598-44-9
methyl 3-bromo-4-cyanobenzoate

Guidance literature:: With N-Bromosuccinimide; palladium diacetate; toluene-4-sulfonic acid; In 1,2-dichloro-ethane; at 70 ℃; for 12h; Sealed tube;
DOI:10.1021/jo302765g

Reference yield: 73.0%

: 143-33-9,25596-52-5
sodium cyanide

: 544-92-3
copper(I) cyanide

: 106896-49-5
methyl 4-amino-3-bromobenzoate

: 942598-44-9
methyl 3-bromo-4-cyanobenzoate

Guidance literature:: methyl 4-amino-3-bromobenzoate; With tert.-butylnitrite; boron trifluoride diethyl etherate; In dichloromethane; water; at -10 - 20 ℃; for 4h;

sodium cyanide; copper(I) cyanide; In water; toluene; at 0 - 60 ℃; for 1.66667h;