3-Chlorobenzenediazonium

Base Information

• Chemical Name: 3-Chlorobenzenediazonium
• CAS No.: 17333-84-5
• Deprecated CAS: 2101457-51-4,2190528-86-8
• Molecular Formula: C6H4 Cl N2
• Molecular Weight: 139.564
• Hs Code.: 2927000090
• European Community (EC) Number: 241-356-9
• DSSTox Substance ID: DTXSID8066187
• Nikkaji Number: J218.124J
• Wikidata: Q81992769
• Mol file: 17333-84-5.mol

Synonyms:3-Chlorobenzenediazonium;17333-84-5;Benzenediazonium, 3-chloro-;EINECS 241-356-9;AZOIC DIAZO COMPONENT 2;Benzenediazonium, m-chloro-;DTXSID8066187;SCHEMBL11574020

Chemical Property of 3-Chlorobenzenediazonium

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 28.15000
• Density: g/cm³
• LogP: -0.17142
• XLogP3: 3.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 139.0063008
• Heavy Atom Count: 9
• Complexity: 137

Purity/Quality:

99% ^*data from raw suppliers

FAST ORANGE GC SALT 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=CC(=C1)Cl)[N+]#N

Technology Process of 3-Chlorobenzenediazonium

There total 3 articles about 3-Chlorobenzenediazonium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-chloro-aniline (108-42-9) → 3-chlorobenzenediazonium (17333-84-5)

Guidance literature:

With hydrogenchloride; sodium nitrite; In water; at 5 - 10 ℃;

DOI:10.1021/ja00288a035

Reference yield:

ethanol (64-17-5) + 3-chloro-aniline (108-42-9) + isopentyl nitrite (110-46-3) → 3-chlorobenzenediazonium (17333-84-5)

Guidance literature:

aus salzsaures 3-Chlor-anilin;

Reference yield:

→ 3-chlorobenzenediazonium (17333-84-5)

Guidance literature:

m-Chloranilin, HBF4, NaNO2;

DOI:10.1021/jo00424a013

upstream raw materials:

ethanol

3-chloro-aniline

isopentyl nitrite

Downstream raw materials:

5-(3-chloro-phenylazo)-quinolin-8-ol

1-(3-chloro-phenyl)-4-((Z)-3-chloro-phenylhydrazono)-5-oxo-4,5-dihydro-1H-pyrazole-3-carboxylic acid ethyl ester

3'-Chloroacetophenone

1,3-bis-(3-chloro-phenyl)-triazene

Refernces

• 1、 Carlson, Brian W.,Miller, Larry L.. "Mechanism of the Oxidation of NADH by Quinones. Energetics of One-Electron and Hydride Routes". . p. 479 - 485. Retrieved 2007/10/02.