Indeno(1,2,3-kl)acridine

Base Information

• Chemical Name: Indeno(1,2,3-kl)acridine
• CAS No.: 386-77-6
• Molecular Formula: C19H11N
• Molecular Weight: 253.2973
• DSSTox Substance ID: DTXSID10191918
• Wikidata: Q83064504
• Mol file: 386-77-6.mol

Synonyms:Indeno(1,2,3-kl)acridine;386-77-6;indeno[1,2,3-kl]acridine;8-azabenzo[a]fluoranthene;DTXSID10191918

Chemical Property of Indeno(1,2,3-kl)acridine

Chemical Property:

• Vapor Pressure: 8.44E-09mmHg at 25°C
• Boiling Point: 476.9°Cat760mmHg
• Flash Point: 215.2°C
• Density: 1.337g/cm³
• XLogP3: 4.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 253.089149355
• Heavy Atom Count: 20
• Complexity: 378

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=CC=C2C(=C1)C3=CC=CC4=NC5=CC=CC=C5C2=C43

Technology Process of Indeno(1,2,3-kl)acridine

There total 4 articles about Indeno(1,2,3-kl)acridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 8.0%

1-azatriptycene (197-45-5) → indeno[1,2,3-kl]acridine (386-77-6) + o-(9-fluorenyl)aniline (75819-53-3) + 12b-methyl-5,12b-dihydroindeno[1,2,3-kl]acridine (74357-31-6)

Guidance literature:

In acetic acid; at 25 ℃; Irradiation;

DOI:10.1021/ja00291a037

Reference yield: 8.0%

1-azatriptycene (197-45-5) → indeno[1,2,3-kl]acridine (386-77-6) + o-(9-fluorenyl)aniline (75819-53-3) + 2H-4a-Aza-benzo[a]indeno[1,2,3-cd]azulene (74368-32-4)

Guidance literature:

In methanol; ethanol; at -196.1 ℃; Irradiation;

DOI:10.1021/ja00543a057

Reference yield: 8.0%

acetic acid (64-19-7,77671-22-8) + 1-azatriptycene (197-45-5) → indeno[1,2,3-kl]acridine (386-77-6) + o-(9-fluorenyl)aniline (75819-53-3) + 12b-methyl-5,12b-dihydroindeno[1,2,3-kl]acridine (74357-31-6)

Guidance literature:

at 25 ℃; for 16h; Irradiation;

DOI:10.1021/ja00291a037

upstream raw materials:

1-azatriptycene

acetic acid

1-azatriptycene

Refernces

• 1、 Sugawara, Tadashi,Iwamura, Hiizu. "Formation of o-(9-Fluorenyl)phenylnitrene in the Photoisomerization of 1-Azatriptycene". . p. 7134 - 7136. Retrieved 2007/10/02.