1-Butylpentylbenzene

Base Information

• Chemical Name: 1-Butylpentylbenzene
• CAS No.: 20216-88-0
• Molecular Formula: C15H24
• Molecular Weight: 204.356
• Hs Code.: 2902909090
• Mol file: 20216-88-0.mol

Synonyms:(1-Butylpentyl)benzene;1-Butylpentylbenzene

Chemical Property of 1-Butylpentylbenzene

Chemical Property:

• PSA: 0.00000
• LogP: 5.15060

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-Butylpentylbenzene

There total 10 articles about 1-Butylpentylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

2-butyl-2-phenyl-hexanenitrile (3508-99-4) + methyl iodide (74-88-4) → 1-butyl-1-phenylpentane (20216-88-0) + C16H26 (56532-96-8)

Guidance literature:

2-butyl-2-phenyl-hexanenitrile; With lithium dihydronaphthylide radical; In tetrahydrofuran; at -40 ℃; for 0.666667h; Inert atmosphere;

methyl iodide; In tetrahydrofuran; at -40 - 20 ℃; for 16h; Inert atmosphere;

DOI:10.1055/s-0030-1258301

Reference yield: 47.0%

ethene (74-85-1) + toluene (108-88-3,15644-74-3,16713-13-6) → heptan-3-ylbenzene (114302-28-2,2132-85-6) + phenylpropane (103-65-1) + pentylbenzene (538-68-1) + 1-butyl-1-phenylpentane (20216-88-0) + (1-ethylpropyl)benzene (1196-58-3)

Guidance literature:

With naphthalene; sodium; lithium; In tetrahydrofuran; at 22 ℃; for 24h; under 760.051 Torr; Inert atmosphere;

DOI:10.1016/j.jorganchem.2008.12.052

Reference yield: 30.0%

ethene (74-85-1) + toluene (108-88-3,15644-74-3,16713-13-6) → heptan-3-ylbenzene (114302-28-2,2132-85-6) + phenylpropane (103-65-1) + pentylbenzene (538-68-1) + heptylbenzene (1078-71-3) + 1-butyl-1-phenylpentane (20216-88-0) + (1-ethylpropyl)benzene (1196-58-3)

Guidance literature:

With stilbene; lithium; In tetrahydrofuran; at 22 ℃; for 24h; under 760.051 Torr; Inert atmosphere;

DOI:10.1016/j.jorganchem.2008.12.034

upstream raw materials:

5-phenylnonan-5-ol

5-phenyl-non-4-ene

1-bromo-butane

benzaldehyde dimethyl acetal

Refernces

• 1、 Rummel,Ilatovskaya,Yunusov,Kalyuzhnaya,Shur. "Activation of C-H bonds of hydrocarbons by the ArH-alkali metal systems in THF (ArH - naphthalene, biphenyl, anthracene, phenanthrene, trans-stilbene, pyrene). Alkylation of naphthalene and toluene with ethene". scheme or table. p. 1459 - 1466. Retrieved 2009/09/06.
• 2、 Azzena,Melloni,Pisano,Sechi. "Single and double reductive cleavage of C-O bonds of aromatic dimethyl acetals and ketals: Generation of benzylic mono- and dicarbanions". . p. 6759 - 6762. Retrieved 2007/10/02.