Technology Process of 3-[1-[3-(Dimethylamino)propyl]-5-methoxy-1H-indol-3-yl]-4-(1H-indol-3-yl)-1H-pyrrole-2,5-dione
There total 5 articles about 3-[1-[3-(Dimethylamino)propyl]-5-methoxy-1H-indol-3-yl]-4-(1H-indol-3-yl)-1H-pyrrole-2,5-dione which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
N,N-dimethyl-formamide;
at 80 ℃;
for 13h;
Heating / reflux;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium tert-butylate / tetrahydrofuran / 12.17 h / 0 - 20 °C
1.2: 1 h
2.1: triethylamine / N,N-dimethyl-formamide / 6.22 h / 0 - 20 °C
3.1: N,N-dimethyl-formamide / 13 h / 80 °C / Heating / reflux
With
potassium tert-butylate; triethylamine;
In
tetrahydrofuran; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triethylamine / N,N-dimethyl-formamide / 6.22 h / 0 - 20 °C
2: N,N-dimethyl-formamide / 13 h / 80 °C / Heating / reflux
With
triethylamine;
In
N,N-dimethyl-formamide;
