Technology Process of Mercury selenide
There total 80 articles about Mercury selenide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
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In
neat (no solvent);
byproducts: 2,2'-selenodipyridine; heated in an evacuated tube at 250°C overnight; XRD;
- Guidance literature:
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In
ethylenediamine;
components (2-8% chalcogen excess) mixing in solvent, stirring at ca. 12°C for 6-16 h; ppt. collection, washing (H2O, EtOH), vac. drying at 80°C for 2 h;
DOI:10.1016/S0022-3697(98)00349-7
- Guidance literature:
-
In
ammonia;
byproducts: NaCl; NH3 (liquid); from HgCl2 and Na2Se in molar ratio 1:1 by stirring at room temp. in liq. NH3 for 36 h; trituration with water and CS2 and annealing at 250°C for 48 h; powder XRD, SEM/EDXA, Raman-, IR-spectroscopies;
DOI:10.1021/ic010648s
