METHYLAMINE HYDROCHLORIDE, [14C]

Base Information

• Chemical Name: METHYLAMINE HYDROCHLORIDE, [14C]
• CAS No.: 34460-70-3
• Molecular Formula: CH₅N*ClH
• Molecular Weight: 69.5073
• Mol file: 34460-70-3.mol

Synonyms:Methylamine-14C,hydrochloride (7CI,8CI);Methanamine-14C,hydrochloride (9CI);

Chemical Property of METHYLAMINE HYDROCHLORIDE, [14C]

Chemical Property:

• PSA: 26.02000
• LogP: 1.07720
• Storage Temp.: 2-8°C

Purity/Quality:

99% ^*data from raw suppliers

METHYLAMINE HYDROCHLORIDE[14C] 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): F,Xi
• Hazard Codes: F,Xi
• Statements: 11-36/37/38
• Safety Statements: 16-26-36

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of METHYLAMINE HYDROCHLORIDE, [14C]

There total 1 articles about METHYLAMINE HYDROCHLORIDE, [14C] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-methyl-14C-phthalimide → 14C-methylamine hydrochloride (34460-70-3)

Guidance literature:

With hydrogenchloride; at 160 ℃; for 16h;

DOI:10.1002/(SICI)1099-1344(199709)39:9<773::AID-JLCR21>3.0.CO;2-1

Reference yield:

14C-methylamine hydrochloride (34460-70-3) + p-toluenesulfonyl chloride (98-59-9) → N-methyl-14C-p-toluenesulfonamide (23826-08-6)

Guidance literature:

With sodium hydroxide; at 80 ℃; for 4h;

Reference yield:

14C-methylamine hydrochloride (34460-70-3) + 6-amino-4-[(3-methylphenyl)amino]quinazoline (153436-70-5) → 1-[4-(m-tolyl)amino-6-quinazolinyl]-3-[14C]-methyl triazene

Guidance literature:

6-amino-4-[(3-methylphenyl)amino]quinazoline; With nitrosonium tetrafluoroborate; In acetonitrile; at 0 ℃;

14C-methylamine hydrochloride; With potassium carbonate; In water; acetonitrile;

DOI:10.1002/jlcr.713

Downstream raw materials:

N-methyl-14C-p-toluenesulfonamide

Refernces