Technology Process of (E)-3-Methyl-2-undecene
There total 17 articles about (E)-3-Methyl-2-undecene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydroxide; dihydrogen peroxide;
cis-dichloro-1,1'-bis(diphenylphosphino)ferrocene palladium(II);
In
tetrahydrofuran;
To a soln. of 9-octyl-9-BBN is added (CH3)2CCHBr, THF and aq. NaOH at room temp., mixt. refluxed overnight (14-16 h), react. mixt. diluted with hexane or benzene, residue oxidized by H2O2 at room temp.; Extracted, washed with brine, dried (MgSO4), final product is identified by mass spectrometry, IR, elem. anal.;
DOI:10.1021/ja00183a048
- Guidance literature:
-
oct-1-ene;
With
9-bora-bicyclo[3.3.1]nonane;
In
tetrahydrofuran;
at 0 ℃;
for 2h;
(Z)-2-Bromo-2-butene;
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium hydroxide;
In
tetrahydrofuran; water;
for 14h;
Reflux;
DOI:10.1021/acs.joc.6b02917
- Guidance literature:
-
With
1-methyl-pyrrolidin-2-one;
iron(III)-acetylacetonate;
In
tetrahydrofuran;
at -5 - 0 ℃;
for 0.25h;
DOI:10.1055/s-1998-2135
![9-octyl-9-bora-bicyclo[3.3.1]nonane](/Databaselist/images/loading.webp)
