8-Chloro-1-methoxynaphthalene

Base Information

• Chemical Name: 8-Chloro-1-methoxynaphthalene
• CAS No.: 41908-14-9
• Molecular Formula: C11H9ClO
• Molecular Weight: 192.645
• Hs Code.: 2909309090
• Mol file: 41908-14-9.mol

Synonyms:8-Chloro-1-methoxynaphthalene

Chemical Property of 8-Chloro-1-methoxynaphthalene

Chemical Property:

• Boiling Point: 303.9±15.0 °C(Predicted)
• PSA: 9.23000
• Density: 1?+-.0.06 g/cm3(Predicted)
• LogP: 3.50180

Purity/Quality:

97% ^*data from raw suppliers

1-Chloro-8-methoxynaphthalene 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 8-Chloro-1-methoxynaphthalene

There total 4 articles about 8-Chloro-1-methoxynaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

CH3O(CH2CHCH2)C6H3(OCOCCl3) → 1-chloro-8-methoxynaphthalene (41908-14-9)

Guidance literature:

C₂₇H₃₇N₂ClCu stable copper(I)-NHC complex; In 1,2-dichloro-ethane; at 200 ℃; for 2h; microwave irradiation;

DOI:10.1016/j.tetlet.2007.12.084

Reference yield: 74.0%

→ 1-chloro-8-methoxynaphthalene (41908-14-9)

Guidance literature:

Reference yield: 10.0%

CH3O(CH2CHCH2)C6H3(OCOCCl3) → 1-chloro-8-methoxynaphthalene (41908-14-9) + (+/-)-8,8'-dimethoxy-1,1'-binaphthyl (82265-47-2)

Guidance literature:

[2,2]bipyridinyl; copper(l) chloride; In benzene; for 1h; Heating;

DOI:10.1016/j.tetlet.2007.09.058

upstream raw materials:

1-Methoxynaphthalene

Downstream raw materials:

8-chloro-1-naphthol

Refernces

• 1、 -. "PROCESS FOR SYNTHESIS OF AROMATIC COMPOUNDS". Page/Page column 12; 14. . Retrieved 2008/06/13.
• 2、 Ram, Ram N.,Tittal, Ram K.,Upreti, Shailesh. "An unusual decarboxylative benzannulation and biaryl formation during copper(I)-promoted halogen atom transfer radical cyclization of 2-allylaryl trichloroacetates". . p. 7994 - 7997. Retrieved 2008/03/14.