Technology Process of Acetic acid phenazin-1-yl ester
There total 8 articles about Acetic acid phenazin-1-yl ester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C16H20N2O2;
With
dichloro[1,3-bis(2-methylphenyl)-2-imidazolidinylidene](benzylidene) (tricyclohexylphosphine) ruthenium(II);
In
ethyl acetate;
at 70 ℃;
for 1h;
Sealed tube;
Inert atmosphere;
With
oxygen;
In
ethyl acetate;
at 70 ℃;
for 4h;
Sealed tube;
DOI:10.1002/chem.202001961
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: diethyl ether / 1.5 h / 0 °C / Reflux
2.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; acetic acid / dichloromethane / 0.67 h / 0 °C
3.1: dichloro[1,3-bis(2-methylphenyl)-2-imidazolidinylidene](benzylidene) (tricyclohexylphosphine) ruthenium(II) / ethyl acetate / 1 h / 70 °C / Sealed tube; Inert atmosphere
3.2: 4 h / 70 °C / Sealed tube
With
dmap; dichloro[1,3-bis(2-methylphenyl)-2-imidazolidinylidene](benzylidene) (tricyclohexylphosphine) ruthenium(II); acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
diethyl ether; dichloromethane; ethyl acetate;
DOI:10.1002/chem.202001961
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; acetic acid / dichloromethane / 0.67 h / 0 °C
2.1: dichloro[1,3-bis(2-methylphenyl)-2-imidazolidinylidene](benzylidene) (tricyclohexylphosphine) ruthenium(II) / ethyl acetate / 1 h / 70 °C / Sealed tube; Inert atmosphere
2.2: 4 h / 70 °C / Sealed tube
With
dmap; dichloro[1,3-bis(2-methylphenyl)-2-imidazolidinylidene](benzylidene) (tricyclohexylphosphine) ruthenium(II); acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
dichloromethane; ethyl acetate;
DOI:10.1002/chem.202001961