1β-Methyl-17β-hydroxy-5α-androstane-3-one

Base Information

• Chemical Name: 1β-Methyl-17β-hydroxy-5α-androstane-3-one
• CAS No.: 1232-57-1
• Molecular Formula: C20H32O2
• Molecular Weight: 304.473
• Mol file: 1232-57-1.mol

Synonyms:1β-Methyl-17β-hydroxy-5α-androstane-3-one

Chemical Property of 1β-Methyl-17β-hydroxy-5α-androstane-3-one

Chemical Property:

• PSA: 37.30000
• LogP: 4.20510

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1β-Methyl-17β-hydroxy-5α-androstane-3-one

There total 4 articles about 1β-Methyl-17β-hydroxy-5α-androstane-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

17β-hydroxy-1-methyl-5α-androst-1-en-3-one (153-00-4) → 1β-Methyl-4,5α-dihydro-testosteron (17β-Hydroxy-1β-methyl-5α-androstan-3-on) (1232-57-1) + mesterolone (1424-00-6)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tributylzinc hydride; In tetrahydrofuran; for 1h; Yield given. Yields of byproduct given; Heating;

Reference yield:

→ 17β-Hydroxy-1α-methyl-5α-androstanon-(3) (1232-57-1,1424-00-6,16662-98-9,56907-08-5,88852-31-7,94901-80-1)

Guidance literature:

17β-Hydroxy-5α-androsten-(1)-on-(3), Methylmagnesiumiodid, CuCl, Diethylether;

Reference yield:

→ (S)-17-Hydroxy-1,10,13-trimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-one (1232-57-1,1424-00-6,16662-98-9,56907-08-5,88852-31-7,94901-80-1)

Guidance literature:

Keton, Grignard;

upstream raw materials:

17β-hydroxy-1-methyl-5α-androst-1-en-3-one

Refernces