tribenzo[fg,ij,rst]pentaphene

Base Information

• Chemical Name: tribenzo[fg,ij,rst]pentaphene
• CAS No.: 190-81-8
• Molecular Formula: C30H16
• Molecular Weight: 376.448
• Mol file: 190-81-8.mol

Synonyms:1,12:2,3:10,11-Tribenzo-perylen;Tribenzo-perylen;

Chemical Property of tribenzo[fg,ij,rst]pentaphene

Chemical Property:

• Vapor Pressure: 3.01E-16mmHg at 25°C
• Melting Point: 380 °C
• Boiling Point: 653.8°Cat760mmHg
• Flash Point: 346°C
• PSA: 0.00000
• Density: 1.401g/cm³
• LogP: 8.63460

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tribenzo[fg,ij,rst]pentaphene

There total 10 articles about tribenzo[fg,ij,rst]pentaphene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

m,m,o,p,o-pentaphenylene (95918-98-2) → 1,12-2,3-10,11-Tribenzoperylen (190-81-8)

Guidance literature:

With iodine; In benzene; for 20h; Irradiation;

DOI:10.1246/bcsj.58.481

Reference yield: 89.0%

1.2-Diphenanthryl-(9)-ethylen (15332-32-8) → 1,12-2,3-10,11-Tribenzoperylen (190-81-8)

Guidance literature:

With iodine; Photolysis; Flow reactor;

DOI:10.1039/c7pp00040e

Reference yield: 77.0%

1,2-diphenyltriphenylene (79421-23-1) → 1,12-2,3-10,11-Tribenzoperylen (190-81-8)

Guidance literature:

With aluminium trichloride; copper dichloride; In carbon disulfide; for 48h; Ambient temperature;

upstream raw materials:

9,12-diphenyl-triphenylene

tribenzo[fg,ij,rst]pentaphene-15,16-dicarboxylic acid-anhydride

Methyl-<9-phenanthryl-methyl>-sulfid

m,m,o,p,o-pentaphenylene

Refernces

• 1、 Hopff,Schweizer. "-". . p. 2315,2323. Retrieved 1959.
• 2、 Zhu, Daqian,Peng, Hui,Sun, Yameng,Wu, Zhouming,Wang, Yun,Luo, Bingling,Yu, Tiantian,Hu, Yumin,Huang, Peng,Wen, Shijun. "Modular metal-free catalytic radical annulation of cyclic diaryliodoniums to access π-extended arenes". supporting information. p. 1972 - 1977. Retrieved 2021/03/26.
• 3、 Mueller, Markus,Mauermann-Duell, Heike,Wagner, Manfred,Enkelmann, Volker,Muellen, Klaus. "Eine Cycloadditions-Cyclodehydrierungs-Route von stilbenoiden zu ausgedehnten aromatischen Kohlenwasserstoffen". . p. 1751 - 1754. Retrieved 2007/10/02.