(2Z)-2-[[2-chloro-4-[3-chloro-4-[(2Z)-2-[2-oxo-1-(phenylcarbamoyl)propylidene]hydrazinyl]phenyl]phenyl]hydrazinylidene]-3-oxo-N-phenyl-butanamide

Base Information

• Chemical Name: (2Z)-2-[[2-chloro-4-[3-chloro-4-[(2Z)-2-[2-oxo-1-(phenylcarbamoyl)propylidene]hydrazinyl]phenyl]phenyl]hydrazinylidene]-3-oxo-N-phenyl-butanamide
• CAS No.: 97794-07-5
• Molecular Formula: C₃₂H₂₆Cl₂N₆O₄
• Molecular Weight: 629.502
• Mol file: 97794-07-5.mol

Synonyms:(2Z)-2-[[2-chloro-4-[3-chloro-4-[(2Z)-2-[2-oxo-1-(phenylcarbamoyl)propylidene]hydrazinyl]phenyl]phenyl]hydrazinylidene]-3-oxo-N-phenyl-butanamide

Chemical Property of (2Z)-2-[[2-chloro-4-[3-chloro-4-[(2Z)-2-[2-oxo-1-(phenylcarbamoyl)propylidene]hydrazinyl]phenyl]phenyl]hydrazinylidene]-3-oxo-N-phenyl-butanamide

Chemical Property:

• PSA: 148.10000
• LogP: 8.09660

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (2Z)-2-[[2-chloro-4-[3-chloro-4-[(2Z)-2-[2-oxo-1-(phenylcarbamoyl)propylidene]hydrazinyl]phenyl]phenyl]hydrazinylidene]-3-oxo-N-phenyl-butanamide

There total 4 articles about (2Z)-2-[[2-chloro-4-[3-chloro-4-[(2Z)-2-[2-oxo-1-(phenylcarbamoyl)propylidene]hydrazinyl]phenyl]phenyl]hydrazinylidene]-3-oxo-N-phenyl-butanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

3,3'-dichlorobenzidine (91-94-1) + N-phenylacetoacetamide (102-01-2,98624-45-4) → C.I. pigment yellow 12 (97794-07-5)

Guidance literature:

With hydrogenchloride; sodium nitrite; In water; at 20 ℃; for 0.333333h; Green chemistry;

DOI:10.1039/c8gc03982h

Reference yield:

C12H8Cl2N4O8S2 + N-phenylacetoacetamide (102-01-2,98624-45-4) → C.I. pigment yellow 12 (97794-07-5)

Guidance literature:

With sodium phosphate; In water; at 5 - 10 ℃; Reagent/catalyst; Concentration; Temperature; Large scale;

Reference yield:

3,3'-dichloro-biphenyl-4,4'-bisdiazonium; chloride (49744-39-0) + N-phenylacetoacetamide (102-01-2,98624-45-4) → C.I. pigment yellow 12 (97794-07-5)

Guidance literature:

With sodium hydroxide; acetic acid; In water; at 20 ℃; for 0.233333h; pH=4.7; Product distribution / selectivity; Industry scale;

upstream raw materials:

3,3'-dichloro-biphenyl-4,4'-bisdiazonium; chloride

N-phenylacetoacetamide

4-(3-oxobutanamido)benzamide

2-acetoacetylamino benzoic acid

Refernces

• 1、 -. "Preparation method of C.I. pigment yellow 12". Paragraph 0051; 0052. . Retrieved 2016/10/31.