5-Chloro-4,5-dihydro-1,4-dimethyl-1H-tetrazaborole

Base Information

• Chemical Name: 5-Chloro-4,5-dihydro-1,4-dimethyl-1H-tetrazaborole
• CAS No.: 21960-49-6
• Molecular Formula: C₂H₆BClN₄
• Molecular Weight: 132.36
• Mol file: 21960-49-6.mol

Synonyms:5-Chloro-4,5-dihydro-1,4-dimethyl-1H-tetrazaborole

Chemical Property of 5-Chloro-4,5-dihydro-1,4-dimethyl-1H-tetrazaborole

Chemical Property:

• PSA: 31.20000
• LogP: -0.88350

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-Chloro-4,5-dihydro-1,4-dimethyl-1H-tetrazaborole

There total 3 articles about 5-Chloro-4,5-dihydro-1,4-dimethyl-1H-tetrazaborole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

methyl azide (624-90-8) + boron trichloride (10294-34-5) + N-ethyl-N,N-diisopropylamine (7087-68-5) → 5-Chlor-1,4-dimethyl-Δ2-tetrazaborolin (21960-49-6)

Guidance literature:

With methylamine; In diethyl ether; 15 h heating at 150°C in tube, than vac. distn.;

DOI:10.1039/DT9720000131

Reference yield:

methyl azide (624-90-8) + methylamine (74-89-5) → 5-Chlor-1,4-dimethyl-Δ2-tetrazaborolin (21960-49-6)

Guidance literature:

With boron trichloride; N-ethyl-N,N-diisopropylamine; In diethyl ether; at 130 ℃;

DOI:10.1039/DT9720000131

Reference yield:

methyl azide (624-90-8) + boron trichloride (10294-34-5) → 5-Chlor-1,4-dimethyl-Δ2-tetrazaborolin (21960-49-6)

Guidance literature:

With triethylamine; methylamine; In diethyl ether; 15 h heating at 150°C in tube, than vac. ditsn.;

DOI:10.1039/DT9720000131

upstream raw materials:

methyl azide

methylamine

boron trichloride

N-ethyl-N,N-diisopropylamine