[1E,5Z,pR]-1,5-Cyclooctadiene

Base Information Edit

Chemical Name:[1E,5Z,pR]-1,5-Cyclooctadiene
CAS No.:5259-72-3
Molecular Formula:C₈H₁₂
Molecular Weight:108.183
Hs Code.:
Mol file:5259-72-3.mol

Synonyms:[1E,5Z,pR]-1,5-Cyclooctadiene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [1E,5Z,pR]-1,5-Cyclooctadiene Edit

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Technology Process of [1E,5Z,pR]-1,5-Cyclooctadiene

There total 142 articles about [1E,5Z,pR]-1,5-Cyclooctadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 55425-72-4
(2,2'-bipyridyl)(1,5-cyclooctadiene)nickel

: 13165-72-5
chlorosulfite de methyle

: 121837-93-2
(bipy)Ni(Cl)(metallasulfinat-Me)

: 998-40-3
tributylphosphine

: 5259-72-3,10060-40-9,111-78-4
cyclo-octa-1,5-diene

Guidance literature:: In tetrahydrofuran; inert atmosphere; cooling soln. of Ni-compd. (-78°C), addn. of org. compd., stirring (room temp.); filtn., washing (hexane), drying; elem. anal.;

Reference yield: 80.6%

: 1295-35-8
bis(1,5-cyclooctadiene)nickel ⁽⁰⁾

: 7440-02-0
nickel

: 13463-39-3,71564-36-8
tetracarbonyl nickel

: 5259-72-3,10060-40-9,111-78-4
cyclo-octa-1,5-diene

Guidance literature:: With carbon monoxide; In hexane; -40°C, warming within 1 h to 0-20°C;

Reference yield: 42.0%

: 108-05-4,9003-20-7
vinyl acetate

: 15133-82-1
tetrakis(triphenylphosphine)nickel⁽⁰⁾

: 74-85-1
ethene

: 100-40-3
4-ethenylcyclohexene

: 373-02-4,14998-37-9,33025-09-1,94044-50-5,98268-31-6
nickel diacetate

: 5259-72-3,10060-40-9,111-78-4
cyclo-octa-1,5-diene

Guidance literature:: In neat (no solvent); under N2 or argon or under vac., excess of org. compd. added to Ni(cod)2 and Ni(PPh3)4 stirred at 25°C for 2 h; detn. by IR and NMR;
DOI:10.1021/ja00413a014