3-DEOXY-D-MANNO-2-OCTULOSONIC ACID, AMMONIUM SALT

Base Information

• Chemical Name: 3-DEOXY-D-MANNO-2-OCTULOSONIC ACID, AMMONIUM SALT
• CAS No.: 20595-77-1
• Molecular Formula: C₈H₁₄O₈*H₃N
• Molecular Weight: 255.225
• Hs Code.: 2923900090
• Mol file: 20595-77-1.mol

Synonyms:KDO

Chemical Property of 3-DEOXY-D-MANNO-2-OCTULOSONIC ACID, AMMONIUM SALT

Chemical Property:

• PSA: 158.35000
• LogP: -4.49240

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-DEOXY-D-MANNO-2-OCTULOSONIC ACID, AMMONIUM SALT

There total 15 articles about 3-DEOXY-D-MANNO-2-OCTULOSONIC ACID, AMMONIUM SALT which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

Oxalacetic acid (328-42-7) + D-lyxose (1114-34-7) → ammonium-2-keto-3-deoxy-D-lyxooctulosonate (20595-77-1,20603-30-9,25539-49-5,103404-70-2,123672-57-1)

Guidance literature:

With potassium hydroxide; In water; for 2h; Ambient temperature;

Reference yield: 18.0%

Oxalacetic acid (328-42-7) + D-ribose (50-69-1) → ammonium-2-keto-3-deoxy-D-ribooctulosonate (20595-77-1,20603-30-9,25539-49-5,103404-70-2,123672-57-1)

Guidance literature:

With potassium hydroxide; In water; for 2h; Ambient temperature;

Reference yield: 17.0%

Oxalacetic acid (328-42-7) + L-arabinose (5328-37-0) → ammonium-2-keto-3-deoxy-L-arabinooctulosonate (20595-77-1,20603-30-9,25539-49-5,103404-70-2,123672-57-1)

Guidance literature:

With potassium hydroxide; In water; for 2h; Ambient temperature;

upstream raw materials:

(R)-3-Hydroxy-5-(1,2,3,4-tetrahydroxy-butyl)-dihydro-furan-2-one

(R)-3-Hydroxy-5-((1S,2R,3R)-1,2,3,4-tetrahydroxy-butyl)-dihydro-furan-2-one

(2S,3S,4S,5S,6R)-2-benzyloxy-6-(hydroxymethyl)tetrahydropyran-3,4,5-triol

phenylmethyl 6-deoxy-6-iodo-α-D-mannopyranoside

Refernces

• 1、 Branchaud, Bruce P.,Meier, Mark S.. "A SYNTHESIS OF AMMONIUM 3-DEOXY-D-MANNO-2-OCTULOSONATE (AMMONIUM KDO) FROM D-MANNOSE VIA COBALOXIME-MEDIATED RADICAL ALKYL-ALKENYL CROSS COUPLING". . p. 3191 - 3194. Retrieved 2007/10/02.