Lanostan-12-one

Base Information

• Chemical Name: Lanostan-12-one
• CAS No.: 52474-77-8
• Molecular Formula: C₃₀H₅₂O
• Molecular Weight: 428.742
• Mol file: 52474-77-8.mol

Synonyms:Lanostan-12-one

Chemical Property of Lanostan-12-one

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Lanostan-12-one

There total 5 articles about Lanostan-12-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

lanostan-11β-ol (54411-50-6) → Lanostan-12-on (52474-77-8)

Guidance literature:

Multi-step reaction with 3 steps

1: POCl₃, Py

2: CrO₃, AcOH / hexane / Heating

3: Li, liq. NH₃

With pyridine; chromium(VI) oxide; ammonia; lithium; acetic acid; trichlorophosphate; In hexane;

DOI:10.1021/ja00809a037

Reference yield:

Lanostan-11-on (50633-28-8) → Lanostan-12-on (52474-77-8)

Guidance literature:

Multi-step reaction with 4 steps

1: LiAlH₄ / diethyl ether / Heating

2: POCl₃, Py

3: CrO₃, AcOH / hexane / Heating

4: Li, liq. NH₃

With pyridine; chromium(VI) oxide; lithium aluminium tetrahydride; ammonia; lithium; acetic acid; trichlorophosphate; In diethyl ether; hexane;

DOI:10.1021/ja00809a037

Reference yield:

lanost-8-ene (6593-21-1) → Lanostan-12-on (52474-77-8)

Guidance literature:

Multi-step reaction with 6 steps

1: CrO₃, AcOH / hexane / Heating

2: Li, liq. NH₃

3: LiAlH₄ / diethyl ether / Heating

4: POCl₃, Py

5: CrO₃, AcOH / hexane / Heating

6: Li, liq. NH₃

With pyridine; chromium(VI) oxide; lithium aluminium tetrahydride; ammonia; lithium; acetic acid; trichlorophosphate; In diethyl ether; hexane;

DOI:10.1021/ja00809a037

upstream raw materials:

Lanost-9(11)-en-12-on

lanostan-11β-ol

Lanostan-11-on

lanost-8-ene