Apocynol A

Base Information

• Chemical Name: Apocynol A
• CAS No.: 358721-33-2
• Molecular Formula: C₁₃H₂₀O₃
• Molecular Weight: 224.3
• Mol file: 358721-33-2.mol

Synonyms:Apocynol A;(4R)-4-[(1E,3R)-3-Hydroxy-1-buten-1-yl]-3-(hydroxymethyl)-5,5-dimethyl-2-cyclohexen-1-one

Chemical Property of Apocynol A

Chemical Property:

• Boiling Point: 377.1±42.0 °C(Predicted)
• PKA: 14.28±0.20(Predicted)
• PSA: 57.53000
• Density: 1.113±0.06 g/cm3(Predicted)
• LogP: 1.45730

Purity/Quality:

98% ^*data from raw suppliers

ApocynolA ≥98% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Apocynol A

There total 2 articles about Apocynol A which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

apocynoside I → (6R,9R)-13-hydroxy-3-oxo-α-ionol (358721-33-2)

Guidance literature:

With β-glucosidase; at 38 ℃; for 24h; pH=4.4;

DOI:10.1248/cpb.49.845

Reference yield: 70.0%

glochidionionoside C → glochidionionol C (358721-33-2)

Guidance literature:

With emulsin; water; at 37 ℃; for 15h; Enzymatic reaction;

DOI:10.1248/cpb.51.286

Refernces

• 1、 Murakami,Kishi,Matsuda,Hattori,Yoshikawa. "Medicinal foodstuffs. XXIV. Chemical constituents of the processed leaves of Apocynum venetum L.: Absolute stereostructures of apocynosides I and II". . p. 845 - 848. Retrieved 2001.